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q21's tek with chacruna? Options
 
biopsylo
#1 Posted : 10/2/2011 4:33:47 PM

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has anyone tried either q21 method-- (limonene or naptha) with chacruna?

if pulling with naptha or heptane from the CaOH, will one run into the problem of the n-oxide being left behind?
 

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dreamer042
#2 Posted : 10/2/2011 4:43:06 PM

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I have done limtek with chacruna and chaliponga salting to fumerates. Limonine works well, I haven't tried naptha but theoretically it should work.
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biopsylo
#3 Posted : 10/2/2011 4:56:19 PM

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nice,
my question arrises from the tendency for the fumarate spice, when pasted out with sodium carbonate and pulled with acetone, only a small portion will come over and evap out of the acetone. this is apparently because the spice in chacruna is mostly n-oxide, which is insoluble in acetone.


edit: checked wiki, and n-oxide is insoluble in naptha, so presumably insoluble in heptane as well.

better off sticking with limonene
 
 
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