A while ago SWIM was making mescaline carbonate using
PlainCoil's method. He go to the point where crude mescaline carbonate was dissolved in hot 99% IPA, and then put in the freezer. However, nothing seemed to be precipitating out. The IPA was dark orange, suggesting that at least some alkaloids were still dissolved in it.
SWIM used roughly 60-70 mL IPA for 1.310 g crude mesc. carbonate (was this too much?) What should SWIM do?
benzyme wrote:
i'm tellin ya, one day i'll interface a mass spec and uv-vis spectrophotometer to a modular synthesizer