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failed process, damage control please... Options
 
mew
#21 Posted : 7/28/2012 8:00:29 PM

huachumancer


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Last visit: 21-Sep-2024
Location: earf
ive evaporated the ipa and it has yielded a black tar

conisdering pulling with dry acetone
 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
jamie
#22 Posted : 7/29/2012 3:05:51 AM

DMT-Nexus member

Salvia divinorum expert | Skills: Plant growing, Ayahuasca brewing, Mushroom growingSenior Member | Skills: Plant growing, Ayahuasca brewing, Mushroom growing

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what does it feel like on your tounge? It will burn on the tounge if it DMT..
Long live the unwoke.
 
mew
#23 Posted : 7/29/2012 10:35:47 AM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
it is a black tar, mew dosent consider putting it on his tongue, there is however a tryptamine smell
 
mew
#24 Posted : 7/30/2012 10:01:41 PM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
dissolved in acetone then filtered, a rusty mud was separated from the acetone solution.

evapping the acetone now
 
mew
#25 Posted : 7/30/2012 10:57:32 PM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
evaporated acetone yielded a dark orange honey smelling strongly of spice
 
mew
#26 Posted : 7/31/2012 1:31:15 AM

huachumancer


Posts: 1285
Joined: 02-Aug-2008
Last visit: 21-Sep-2024
Location: earf
since there are previous spice saturated steps (my desire to find a way out of my mess lead me to unfinished steps, leaving behind valuable spice) im going to consolidate it all.

the conversion to freebase using washing soda will be pulled with dry acetone (i ran out of dry ipa to continue pulling)
all paper towels that i used to clean up dishes/tools/hands will be pulled with dry acetone
all filters and cotton balls will be pulled with dry acetone

all acetone will be combined and evaporated

the resulting product will be acidified and filtered
this product will be evaporated

the final unseparated salt that was acetic was bassified (had crazy emulsions anyway)
it will be pulled 3 more times, combined, and salted with fumaric acid solution (4x)

the previous fumaric acid solution will be combined with the final salting and evaporated

the product yielded will be dmt fumarate.

whew.... glad this is over Smile

half the fumarates are going to be converted to fb, the other half will have the excess fumaric acid removed to use as insufflated fumarates/ pharma



 
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