Hi

This is my second extraction from acrb (50gr) following cyb salt tek and mini a/b from Earthwalker.

I use hexane for the pulls, i have to weight it and i want to use in changa with a 10x caapi leaf and maybe some others herbs.

I've made mistake in this extraction: loose some solvent in the pulls separation, not be able to separate all the hexane in the first step of mini a/b, plus, the acid solution of 50gr was divided in two container, processing the first that end in a goo, then the other 25gr remain in the fridge for weeks, then extracted and before the mini a/b put togheter the two extract....chaos....but funny.

The crystal are white (the yellow is from photo light) but not really solid, a little white goo (maybe some oils from the first step in mini a/b), i like hexane, but read a little about toxicity and my freezer smell a little of solvent :-( contamination....and fear, poor equipment....is possible that i switch in a nontoxic or lesstoxic tek in the future try, also i don't need crystal and i like the goo / full spectrum.

Did you have to tell me what nontoxic tek can be good for a unexperience people like me ?
Thank to all :-)

....ok, the more solid part that i was able to scrape is 0,475 gr...now i wait the other goo that remains on the glass, i put some warm ethanol and transfer to a container that i weight before when it's evaporate i see the diffrence so i think 0,500 gr from a chaotic acrb extraction....it's a good result ?

Not a bad result for 50g of acrb, looks clean. Check out endlessness ethanol sodium carb and vinegar tek, or you can just substitute the naptha for limo, do a mini acid-base on the limo using fumaric acid or vinegar and convert to freebase using paste and pull with dry ethanol/ISO/acetone.

Thanks i start to read and understand some of non toxic tek and i have to read more on fumaratic, is a thing that i don't know at all...i can't evaporate the limo and have a goo ? i can use it for changa....if i want xtals i can use toxic solvent, maybe when i'm more experience and have at least a room that i can use for thing like this, maybe put some aspirators....ok, it's something that i do in my work when i varnish my woodworking things...i don't know if it's more toxic a little hexane or poliuretanic varnish an solvent....ok now i can enjoy what i get, the next time will be different, thank, really good people here, i like it :-)

Though I've never used limo, apparently you can't evaporate it. You'd need to convert the DMT freebase to it's fumaric salt form to precipitate it from the limo.

After this, you can convert it back to freebase should you choose to vaporize it.

no, dont evap limo, salt it out with FASI/FASA, then dissolve in water and base it with Sodium Carb.


you get crystals using Limo and the FASI/FASA method



Limo extract is mainly DMT, check out endlessness' work, i think its about 98%+ DMT.

Thanks,
So the route is use limonene and FASI/FASA, then convert to freebase, ok, maybe the next time i can try it.

I think i my area it's very difficult to find limonene, but i never searched well.