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Jorkest's D-Limonene Bufotenine Extraction TEK Options
 
WSaged
#261 Posted : 5/23/2009 3:54:56 AM

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Nice!

Ya know, that's another thing, I've not thought my extract was all that harsh on the lungs. I tend to take weenie hits when I'm expecting something harsh, so it may just be me...and that may also be why I've have not gotten any great effects too.
Especially when we soaked some Bufo-tone into a joint, it was just like smoking a joint, except the obviously stronger body buzz.

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soulfood
#262 Posted : 5/23/2009 4:08:27 AM

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I tried smoking it slowly but didn't get anything beyond a tingle. I had to really punish myself to get a load in. I think with this stuff it's always going to be pretty damn hot. Even with my last extract there was zero nausea and barely any vasoconstriction, so the toxins couldn't have been all that prominant.

I now smoke it the same as my DMT on ash in a bong, but like in Ron's test tube vape I let it sit for a minute, problem is my hands aren't big enough to cover all the hole efficently. I may have to invest in some clamping equipment.


One more thing... I'm now just heating to 150 and because the limonene isn't hot enough to evap slightly on contact with the glass when pouring out, the bufo isn't sticking to it as before. The crystals are so tiny, they just float around and it's almost impossible to decant, even with my tiniest pipette.

I'm flirting with the idea of pouring the bufo/limo through a cotton filter, letting it dry and then washing the cotton with acetone to retrieve the goods.

Anyone got a better idea?
 
Garulfo
#263 Posted : 5/23/2009 1:41:59 PM

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Quote:
I'm flirting with the idea of pouring the bufo/limo through a cotton filter, letting it dry and then washing the cotton with acetone to retrieve the goods.

Anyone got a better idea?


Why not add some acetone to your limonene ? Acetone will catch the bufo and is non soluble in limo, so you can separate them easily. Then evaporate your acetone...
 
soulfood
#264 Posted : 5/23/2009 3:40:50 PM

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I thought acetone was miscible in limonene?

Well it is in xylene and I generally treat the 2 as the same.
 
Jorkest
#265 Posted : 5/23/2009 5:47:12 PM

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actually it may not be...to test it out..just get some clean d-limo..and some acetone and see if they mix
it's a sound
 
soulfood
#266 Posted : 5/23/2009 6:58:18 PM

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yup... merged like good n's.

Gonna leave it for a bit just in case of late seperation but it doesn't look hopeful. Probably would make a funky cologne though so let's not sell it short.


Anyways 200g's of seeds, 5 litres of acetone, much mixing, drying and finger tips so burnt they've grown a crispy shell... I finally have something I wouldn't describe as brown.

Havent weighed it. It's quite fluffy so I'm guessing no more than 70mg.

No going straight to bioassay this time... must prepare carefully for this because I'm not sure if I can stomach the whole process again right now. Maybe in a month or two.

From here on it's all about keeping ears to the ground for uber potent strains.

Getting a gram from 50g's of seeds seems like a fantasy right now but some day, hopefully Smile
 
Jorkest
#267 Posted : 5/23/2009 8:13:05 PM

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HMMM!! if the acetone merged perhaps you can do something similar to MEK:heptane...except you would just do d-limonene:acetone the acetone would evaporate off..and the bufo should drop out..then you may be able to wash it with something like heptane to get any d-limo off of it..
it's a sound
 
soulfood
#268 Posted : 5/23/2009 9:32:33 PM

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soulfood wrote:


Anyways 200g's of seeds, 5 litres of acetone, much mixing, drying and finger tips so burnt they've grown a crispy shell... I finally have something I wouldn't describe as brown.




Especially now... because it went black Sad

I quit.
 
Jorkest
#269 Posted : 5/23/2009 9:34:23 PM

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bufo extractions are such a bitch...especially when you get bunk seeds...better luck next time dude
it's a sound
 
soulfood
#270 Posted : 5/23/2009 9:43:57 PM

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Yeah the timing is lame.

Lost my job a while back, which I wasn't too bothered about but as I'm having trouble finding another it means back to my folks place for a couple of months until I find my feet... no extracting there Sad
 
Jorkest
#271 Posted : 5/23/2009 9:56:00 PM

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damn dude...that sucks...well...just remember...you wont forget how to do all this stuff..so as soon as you get a new place..you can start right back up..just make sure you come to the site and stay up to date...dont want to miss anything good
it's a sound
 
soulfood
#272 Posted : 5/23/2009 10:04:53 PM

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Oh of course.

I'll still be extracting mesc and spice on the sneak if needed and I'm sure a friend wouldn't mind inviting me round to cook... it's just this one extraction is pretty difficult to hide/transport.

All those memories of growing mushrooms on top of my cupboard when I was 17 are all flooding back to me Smile
 
Garulfo
#273 Posted : 5/23/2009 10:26:40 PM

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I'm surprised about acetone/limo... SWIM added some limo in some bufo+acetone and there was distincly two layers, but maybe it is because there was some bufo (dark amber color) in the acetone...
You may also try with ethanol.
 
Jorkest
#274 Posted : 5/23/2009 10:34:33 PM

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hahaha nice dude...
it's a sound
 
SpasticSpaz
#275 Posted : 5/27/2009 9:22:42 PM
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Am I allowed to post a supplier in this thread? SWIM told me of one that he just received, which gave him light OEVs on smoking the seeds straight, something that's never happened with any other supplier's stuff, and he really wants me to share the supplier here. Can I?
 
Garulfo
#276 Posted : 5/27/2009 10:50:52 PM

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I'm interrested in knowing that supplier by PM....
 
soulfood
#277 Posted : 5/28/2009 11:49:55 AM

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Me too Smile
 
Garulfo
#278 Posted : 5/28/2009 1:19:19 PM

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Thanks for the link.
Edit: I was wrong, they are not that expensive.
 
Phlux-
#279 Posted : 6/7/2009 7:18:26 AM

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please pm me that vendor someone.
antrocles wrote:
...purity of intent....purity of execution....purity of experience...

...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


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‹Jorkest› the wall is impenetrable as far as i can tell


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He who packs ur capsules - controls your destiny.

 
Trips
#280 Posted : 6/24/2009 10:33:43 PM
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meeee toooooo.
 
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