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Edit: Results: A/B of 50g yield vs old STB yields (same batch). Options
 
Silly(c)One
#21 Posted : 4/10/2013 3:39:45 AM

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Orion wrote:
Quite pleased with these results.

That's the only thing that matters after all, isn't it Very happy
Beautiful crystals indeed, very nice job ! Smile

Sure, acid extractions only make sense with bigger amounts of bark, just like STBs are better fitted to lower amounts.

So, which method did you prefer doing ?
 

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Orion
#22 Posted : 4/12/2013 12:47:50 AM

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Well in this case I believe numbers speak for themselves, as others also seem to agree by comparison for example. https://www.dmt-nexus.me...&m=170401#post170401

Perhaps more direct comparisons might be tallied up to get a better idea if one really is better than the other, or if it is just chance, but I find that unlikely if the bark used is from the same batch with the same solvent.

(There is still more crystallizing in heptane, a very small but I believe significant amount for this yield)
Art Van D'lay wrote:
Smoalk. It. And. See.
 
Orion
#23 Posted : 4/12/2013 1:27:57 AM

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EDIT: Whoops hit the button, kikker made me do it.
Art Van D'lay wrote:
Smoalk. It. And. See.
 
Silly(c)One
#24 Posted : 4/12/2013 5:19:44 AM

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I meant, which tek do you prefer executing ?

With a bit of practice, one can get very similar results with A/B and STB, so I was more interested in your thoughts and impressions than numbers Smile
 
Orion
#25 Posted : 4/12/2013 8:00:04 PM

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Though much of my method after the boils is exactly the same as the way I do an STB, I prefer this because it's less messy. Getting dry pulverized bark into the thin bottle stem is such a pain, but not when it's a hydrated sludge.
Art Van D'lay wrote:
Smoalk. It. And. See.
 
Silly(c)One
#26 Posted : 4/13/2013 2:25:21 PM

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Are you using a funnel ? Just a thought Pleased
 
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