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psychosisdoses
#1 Posted : 3/20/2009 12:59:02 AM

Derek


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they are dry but still taste iv used this acetone before no problem suggestions?
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Jorkest
#2 Posted : 3/20/2009 2:18:58 AM

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if you can still smell or taste the acetone..try putting them on a flat piece of glass and chopping them up over and over again with a razor blade...SWIM does this to get most of the d-limonene out of his bufo..it takes awhile..but its easy..so just give it a try
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psychosisdoses
#3 Posted : 3/20/2009 4:17:18 PM

Derek


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Jorkest wrote:
if you can still smell or taste the acetone..try putting them on a flat piece of glass and chopping them up over and over again with a razor blade...SWIM does this to get most of the d-limonene out of his bufo..it takes awhile..but its easy..so just give it a try



yup thats the method iv been using.... i got alot of crystals tho heh heh heh
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
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psychosisdoses
#4 Posted : 3/26/2009 4:17:45 AM

Derek


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i got an idea... would dissolving in a small amount of water and evaping the water work??
iv choped them the best i can and continue doing so but it seems less then effective
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
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psychosisdoses
#5 Posted : 4/7/2009 1:54:34 AM

Derek


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i have found that crushing with a blunt object and chopping to remove most taste... you can sometimes smell solvent the first crush or two... i have dissolved a small amount in water and am now evaping the water in a dish ill update whenever the water dries and i taste it... seems to me this would work quite well at removing any trace solvent but we shall see....
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
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downwardsfromzero
#6 Posted : 4/19/2009 9:24:23 PM

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Hope your recrystallisation worked...




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geeg30
#7 Posted : 4/20/2009 2:30:47 AM

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Why don't you redissolve in hot naptha and then evap that, the acetone will evap before the naptha does?
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psychosisdoses
#8 Posted : 4/20/2009 3:55:43 AM

Derek


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well they tasted a bit less like acetone but still did... i wasnt aware furmate salts were soluble in naphtha am i mistaken?
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
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geeg30
#9 Posted : 4/20/2009 2:55:49 PM

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Ahh I thought you had freebased them. Sorry
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psychosisdoses
#10 Posted : 4/20/2009 10:35:40 PM

Derek


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geeg30 wrote:
Ahh I thought you had freebased them. Sorry


its quite alright.. i had infact freebased them Pleased but then i salted them out with FASA.

i may just decide to use the furmate as storage and convert back to freebase as needed because i never had this problem with freeze perciped freebase
"once youve locked yourself into a serious drug collection the tendency is to push it as far as you can..." - hunter s. thompson

~~~~~~~~...You are me and i am you, i will always be with you...~~~~~~~~IAmUsWeYouMe~~~~~~~~
‹maxzar100› YOU are like acid
‹mattimus› dosesdosingdoses
 
shoe
#11 Posted : 1/27/2010 1:41:28 PM

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The good people at the nexus have seen to you it seems Smile
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amor_fati
#12 Posted : 1/27/2010 4:24:35 PM

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No matter what SWIM did, if FASA retrieved fumarate were left in a sealed container for a while, once that container was opened, the odor of acetone was emitted. Once, SWIM was certain that he had removed all of it by crushing it and took it orally, and later, he burped up a bit of acetone. The only reliable way to remove traces of acetone is anything along the lines of this. SWIM'll be doing a more generalized writeup of this purification procedure in the near-future.


Edit:
and here it is: Wiki Article for Purification of Spice Fumarate Product
 
 
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