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Manske->Methanol->Goo->Huh? question Options
 
Pup Tentacle
#1 Posted : 1/20/2013 3:54:19 PM

lettuce


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So I did the old Manske plan on some rue and had a nice little pile of "sparkling dirt".

** The tek for reference-> https://wiki.dmt-nexus.m...Crystals_from_Syrian_Rue **

I then mixed in some methanol (per the tek), filtered through a coffee filter into my glass baking pan, let it evap (95% dry) and then...(not per the tek) I put it in a 250˚F oven for about 20 min to give it some evaporation boosting.

Now I have goo that's like a brown candy-ish consistency but it still flows (albeit too slowly to see).

Did I wreck the plan by adding heat to the equation? Should I just redissolve in methanol and leave to evap without heat?

All advice appreciated. Thanks Smile

PT

Magic goo pictured below...
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Pup Tentacle

You are precisely as big as what you love and precisely as small as what you allow to annoy you.
Robert Anton Wilson
Mushroom Greenhouse How-To
I'm no pro but I know a a few things - always willing to help with Psilocybe cubensis cultivation questions.
 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
Shadowman-x
#2 Posted : 1/20/2013 5:08:32 PM

x-namwodahs

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You should be fine. You can dissolve and re-manske the xtals to get nicer ones.
They don't think it be like it is, but it do.
 
Pup Tentacle
#3 Posted : 1/20/2013 5:56:20 PM

lettuce


Posts: 1077
Joined: 26-Mar-2012
Last visit: 15-Jan-2016
Location: Far, Far Away
right on, thanks - this is still a salt right? impurish harmala hcl?

Might there be an easy path to FB with my goo? Dissolve in h2O - add base (maybe some ammonia)- would that precip FB harmalas?
Pup Tentacle

You are precisely as big as what you love and precisely as small as what you allow to annoy you.
Robert Anton Wilson
Mushroom Greenhouse How-To
I'm no pro but I know a a few things - always willing to help with Psilocybe cubensis cultivation questions.
 
 
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