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Silicon in solvent Options
 
TimePantry
#1 Posted : 6/6/2012 12:01:54 AM

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A small silicon gasket fell into my solvent and, apparently, dissolved. I didn't notice it missing until later on, after I had poured the solvent into some MHRB mud. Heh, that explains that permanent emulsion. Dammit.

Anyway my question is, solvent being somewhat hard to come by in my state, can it be salvaged? And has the silicon fouled my whole batch? (I am assuming so.) Will it just stay in solution in the solvent? Will it precipitate out along with the spice?

Anything you can tell me is very much appreciated.
"What's wrong with that generation? ... Is this what comes of putting on Pink Floyd laser lightshows down at the Planetarium?" --Spider Robinson
 

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InMotion
#2 Posted : 6/6/2012 5:01:56 PM
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What I would try to do is take the tainted solvent and perform a few acid washes on it(vinegar or other dilute acid). Then basify again into clean solvent. Silicon should not come out of a freeze precipitation, but a re-x sounds like a good idea after anyways.

Distillation would recover your solvent without 'silicon' impurities though this is not an option for many.
 
TimePantry
#3 Posted : 6/6/2012 5:40:24 PM

It's a field.


Posts: 230
Joined: 26-Jun-2011
Last visit: 29-Oct-2019
Hey, thanks! That's an enormous relief. I've been seriously worried that the resulting spice would be deadly or something; I shelved it all until I could find out.

I notice you put 'silicon' in halfquotes -- am I using the term incorrectly?


(p.s. love your tagline.)

Whoops, wikipedia straightened me out -- "silicone."
"What's wrong with that generation? ... Is this what comes of putting on Pink Floyd laser lightshows down at the Planetarium?" --Spider Robinson
 
 
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