CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Passion flower extraction questions Options
 
Dorge
#1 Posted : 10/18/2011 11:25:20 PM

Chen Cho Dorge


Posts: 1781
Joined: 30-Dec-2008
Last visit: 25-Nov-2012
What would be the best method for extracting the harmalas from passion flower and isolating them?
Dorge is cooperatively owned and cooperatively run by various hyperspacial entities working as a collabertive sentience project for the betterment of sentient exploration.

Offical Changa web sitehttp://changa.esotericpharma.org/


 

Explore our global analysis service for precise testing of your extracts and other substances.
 
nen888
#2 Posted : 10/19/2011 3:45:34 AM
member for the trees

Acacia expert | Skills: Acacia, Botany, Tryptamines, CounsellingExtraordinary knowledge | Skills: Acacia, Botany, Tryptamines, CounsellingSenior Member | Skills: Acacia, Botany, Tryptamines, Counselling

Posts: 4003
Joined: 28-Jun-2011
Last visit: 27-May-2024
..i would recommend ethanol/mild acetic acid (with some heat X3), basification, then non-polar extraction..
there is some good information in this old paper:
partition coefficients of ether extractable passionflower alkaloids
..most recorded herbal usage and chemical tests have been with stem or leaf,
i'm not sure if the actual flowers have ever been analysed ironically...

 
nen888
#3 Posted : 10/20/2011 4:45:59 AM
member for the trees

Acacia expert | Skills: Acacia, Botany, Tryptamines, CounsellingExtraordinary knowledge | Skills: Acacia, Botany, Tryptamines, CounsellingSenior Member | Skills: Acacia, Botany, Tryptamines, Counselling

Posts: 4003
Joined: 28-Jun-2011
Last visit: 27-May-2024
the above linked paper by Eskil Hultin (1960) says the following in the Experimental

Quote:
The portion of the ethanol extract of Passiflora incarnata which was soluble in dilute phosphoric acid was made slightly basic with sodium hydroxide and then extracted continuously with ether for several days...Only small amounts alkaloids were extracted...(Further continuous extraction with a mixture of methylene chloride and methanol over a period of a week yielded an extract considerably higher in alkaloid content.)

..the paper also gives information for the separation of various ß-carbolines from eachother,
and from phenols, using buffer solutions at different pH..methylene chloride is dcm..
as the water soluble flavinoids may also be responsible for activity, one may not necessarily
want to discard these, and water soluble fractions could also be solidified/purfied..
.
[EDIT - ps. the above quote suggests full spectrum solvents like xylene or d-limonine should be used, not napatha.]
 
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.021 seconds.