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WalktheLongRoad
#1 Posted : 3/21/2011 12:37:45 AM

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Joined: 20-Mar-2011
Last visit: 15-Apr-2011
...WalktheLongRoad says Hello!

Like many others, I've been coming back to this site again and again; more recently lurking and absorbing the wealth of information it and everyone here, has to provide! Thank you for creating such a wonderful and active community!

Shamanism and ayahuasca, as well as DMT and other psychedelics have held my interest for a while. I have dabbled some with cannabis, mushrooms, and lsd, but not enough to claim I'm very experienced with them.

I want to begin working with spice, and eventually ayahuasca. There are some things about myself I know I need to face, some emotional and spiritual obstacles I need to overcome, and it is for that reason I am both looking forward to the experience and somewhat fearful of it (as I feel I will be dealing with fear then). But I am hopeful too that as an artist, I might find new and powerful inspiration from it.

Over the last few days I had a sort of spark of productivity and actually tried my first DMT extraction using Q21Q21's A/B lime tek. Here's a brief overview of how it went:



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I used tek 2 with 80g MHRB, did 3 pulls and left them overnight and half a day to freeze precipitate. The second pull yielded the most, the third was the smallest. I unfortunately was not able to do a 4th pull the next day; but I did get to relearn some things from my glassblowing class Confused

I used a 1 quart mason jar to mix everything in, which worked fine for the initial 3 pulls, as the chemical reaction had sufficiently warmed it to prevent heat shock when exposed to the near boiling water in the surrounding bowl. When I went to do the 4th pull though, the jar was cool and so I ended up with "pop" "crack" and a pile of mimosa mud and a jar without a bottom.

I did save all of my naptha (I used a fresh batch for each pull) and I am in the process of evaporating it down slowly, either all the way or to freeze again.

My total product so far is ~0.296g of fluffy white crystals just like those pictured in the tek. Which, even if I don't manage to get anymore out of it, I'm perfectly happy with for my first attempt. I think if it weren't for my mishap I would have been at or around 0.5% yield.


I learned a lot about the process though, and definitely noted a few useful points for the future:
- pyrex is the way to go
- a funnel or two would be a great help
- 1/2 pint jars are nice for precip, but only if you don't tilt them. I had a fair amount of crystals trapped on the upper surfaces inside, and I eventually just gave up and rinsed the jars with my leftover naptha, in hopes of getting it back later.

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I don't have a vehicle to test any of it yet, nor do I want to rush into it. Maybe I'll be more ready when I get (or make) something proper. I look forward to it!

As I look forward to my time here with all of you at the nexus Smile
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WalktheLongRoad does not exist, any events or activities described by this character are fictional and provided for entertainment purposes only.

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STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
endlessness
#2 Posted : 3/21/2011 7:24:46 PM

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Welcome to the Nexus!

Congrats on getting something out of your first extraction! though under 300mg from 80g bark is not such a good yield, is the bark from a good source? Or indeed there will be more crashing out if you evap some more and freeze again (or evap it all down and re-crystallize the goo that will probably remain.

Tell us when you do try vaporing it.. Good luck!
 
Ice House
#3 Posted : 3/21/2011 7:36:40 PM

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Welcome!
Ice House is an alter ego. The threads, postings, replys, statements, stories, and private messages made by Ice House are 100% unadulterated Bull Shit. Every aspect of the Username Ice House is pure fiction. Any likeness to SWIM or any real person is purely coincidental. The creator of Ice House does not condone or participate in any illicit activity what so ever. The makebelieve character known as Ice House is owned and operated by SWIM and should not be used without SWIM's expressed written consent.
 
WalktheLongRoad
#4 Posted : 3/22/2011 2:58:50 AM

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Last visit: 15-Apr-2011
Thank you both for the welcome!

endlessness- I got my bark from heavenly products, they seem reputable though I don't really know for sure. I have another 150g left, and I'm thinking of doing three separate extractions to prevent loosing all of it if something goes wrong, and so that I get more practice. I'm going to freeze my leftovers tonight so between that and my future attempts I should be able to tell whether the it was the bark itself or me that caused the low yield!

I also may end up trying the spice sooner than I anticipated. While looking over the designs posted in the wiki for various administration devices, I realized I pretty much had everything I needed to make one and I love making things...

So, I basically constructed a bubbler using a mason jar some rubber and vinyl tubing, and then made "The Inspirator mkII" for the stem. I don't know yet when I'll use it, but I will certainly post how it goes.




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WalktheLongRoad does not exist, any events or activities described by this character are fictional and provided for entertainment purposes only.

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WalktheLongRoad
#5 Posted : 3/24/2011 4:52:25 PM

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Joined: 20-Mar-2011
Last visit: 15-Apr-2011
Update: After evaporating down and refreezing the leftover naptha, I got another 0.179g, so that brings the total yield for the first extraction up to 0.475g. I think that's a bit more on track, but I'll see if I can't do better next time.
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WalktheLongRoad does not exist, any events or activities described by this character are fictional and provided for entertainment purposes only.

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Another Rube
#6 Posted : 3/24/2011 9:46:33 PM

Nublet will do.


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Oh wow multiple extractions from just one source, so obvious! Haha thank you so much! XD

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