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Soxhlet and Fine Powder Options
 
Trickster
#61 Posted : 12/7/2010 5:10:42 PM

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Shaolin wrote:
Unwarranted as in, not being selective, alkaloid wise ?


Meaning, not giving any increase of spice yield. Of course, it could be very useful for full spectrum extraction.

Shaolin wrote:
I'm not convinced about the need for some many pulls. I think you should monitor invidually. Could be that the first pull yield 450, the second one 100, and the other four 20 total.


That's a good idea for my next experiment.

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Trickster
#62 Posted : 12/7/2010 5:14:33 PM

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benzyme wrote:
DCM can't unbind the alkaloids from intracellular macromolecules, that is, it doesn't hydrolyze DMT from other intracellular molecules.


Am I right thinking that alcohols can?
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benzyme
#63 Posted : 12/7/2010 7:10:22 PM

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well, sort of

but alcohols will not change the charge state of the terminal amine, the primary reason we do
A/B. this separates the alks from other molecules like plant carbohydrates.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
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