for this tek you need:
Quote:Big caustic-proof container, Big Saucepan, 2-4x500ml Beakers, 2x250ml Beakers, Funnel, Separation Funnel
White vinegar, Lye (>98%), Naphtha (or equivalent solvent), pH papers, a Clear Mind, and Accuracy
~
Measure 100g of of MHRB, set it aside. Pour
1.4L of distilled water into a big saucepan and add 150ml of white vinegar - check pH, if its
2-3pH that's good. Add a little more and check again until you're happy.
~
Add the MHRB powder to the water slowly using a fork to mix it all in thoroughly, then boil it for an hour. Always keep it mixed well, tend to it regularly (every 40 seconds or so)
~
Decant that and set aside
~Add another
1.2L of
2-3pH acidic water, it has to be distilled water (used for ironing)
~
Cook for another
30 minutes
~
Decant and
add to the rest of the source fluid
~Put all of this into a funnel with a
Charmin filter in the spout. You will position this over the top of a large acid safe container that has got
10mm of naphtha at the bottom. [Reminder: Use a piece of
cut up shirt to squeeze all the liquid from the acid cook from the powdered bark, discard plant material]
!:
Appendix:: Charmin filter: a Charmin filter is 2 (3 for big funnels) squares of toilet paper which are folded then rolled into a cylinder which fits the spout of your funnel.
~After
filtration is
complete use your separation funnel to discard the naphtha (i cant stress enough how important accuracy is in separating properly and getting rid of everything you don't want)
~Now that you have a high quality
source fluid you should put it into a clean saucepan, boil it to
reduce the volume to around
1L all up (this will make it easier to extract)
~Now you should
add your lye, but don't just add it directly to the source fluid, this can cause Glass to crack and end in disaster. Instead, mix 50g into 200ml distilled water,
adding slowly. Now after that's done
let it cool. Then add it to the source
slowly. Stop adding it when the mixture stops clouding up and is completely black. pH should be around 13
~Now
add naphtha and
source liquid into a
separation funnel at ratios of about
1:10 Naphtha:Source liquid
~
Shake the Separation funnel vigorously for 8 minutes and then let it
settle (swirl it around occasionally if it wont separate).
~
Pour off the Source liquid, making sure to get rid of as much of the source liquid without losing naphtha.
Keep the source liquid in a beaker and set it to the side (label it if you have to)
~Do this for the
total source liquid.
This is pull #1~
Repeat previous step another 2 times
~Now that you have DMT containing Naphtha, cover the beaker with glad wrap and poke a small hole at the top with a pin. Place this in the freezer and don't check it for 18 hours+
~Remove it from the freezer and pour off the naphtha and keep it to evaporate. Break all the chunks off the beaker and spread it out on a plate. Allow to dry for a few days.
~
Scrape it up and weight it.______________________________________________________________________________________________________________
Pictures to come in the future.Please comment on any part of the technique. could this be developed further?
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