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ismokecrystals
#1 Posted : 1/28/2010 10:57:16 PM

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I am attempting the non-toxic extraction of cactus using d-limo and hydrated lime

Right now I have a "warm milkshake" consistency liquid. I used a strainer to filter out the solids as best as possible but it seems there is an emulsion of some sort with the limonene and cactus/lime/water.

Is this salvageable as-is? can I add water to dilute and filter through coffee filter?

If not, can I further basify the solution with NaOH and extract the alkaloids with naptha?

After that for the acid wash, would I have to find a stronger acid than 5% acetic acid?

Any pointers are helpful!
 

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Nordic
#2 Posted : 1/30/2010 5:41:56 PM

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I'm by no means an expert but I had a similar thing happen to me this week, except I used lye as a base.
I ended up makeing a little bit of higly concentrated lye and water and added it to my gel locked bottle then shook it up, and it started seperating pretty nicely, still a tiny emulsion layer (probably lipids from when the pH dipped too low- the xylene/solvent then is basicaly a defat, as far as I think), but 95 of the xylene gets through it pretty fast. As opposed to doing nothing for two days before I base bombed it.

Maybe one of the clever people can say if it will suit your solvent etc...
 
ismokecrystals
#3 Posted : 1/31/2010 7:03:17 PM

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I should be able to basify the solution with a bunch of NaOH and then add xylene. I could then continue with muriatic acid like in conventional teks.

Anyone have comments?
 
Phlux-
#4 Posted : 2/1/2010 5:43:49 AM

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mesc is insoluble in naptha - use the xyelene.
add a bit more water and more lye.
use 4 drops of 33% hcl in 100ml water to salt.
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...unlike the "blind leading the blind". we are more akin to a group of blind-from-birth people who have all simultaneously been given the gift of sight but have no words or mental processing capabilites to work with this new "gift".

IT IS ONLY TO THE EXTENT THAT WE ARE WILLING TO EXPOSE OURSELVES OVER AND OVER AGAIN TO ANNIHILATION THAT WE DISCOVER THAT PART OF OURSELVES THAT IS INDESTRUCTIBLE.


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