We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
123NEXT
Bufotenine... Success..... Maybe? Options
 
LucidLemonade
#1 Posted : 1/14/2010 1:47:36 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
SWIM may have just had some success with a bufotenine extraction...

He was trying one of the other TEKS which again after toasting the extract turned to a black oily mess that he couldn't seem to then pull anything good from.

After that attempt failed he still had left over 50ml of 99% IPA that had been pulled from the based seeds... So he then went to step 4 below...

1. Grind seeds
2. Base with Sodium Carbonate...
3. Pull with IPA.
4. Get another equal amount of IPA and saturate with furmic acid.
5. Add Furmic Acid IPA to the pulled seeds IPA.
6. lots of precipitation.
7. pour off reaming IPA.
8. Base precipitation again with Sodium Carbonate.
9. pull with Acetone.
10. evap onto plate to get a nice light tan coloured crunchy powder..

This is the first time SWIM has gotten anything near to a nice solid crunchy powder....

Basically it's FASA but use IPA instead of Acetone.... As reports seem to indicate that IPA pulls a lot less of the nastiest that Acetone..

SWIM now has 100mg of this TAN powder which he hopes to Bio-essay later tonight...

Fingers crossed.....
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 

Explore our global analysis service for precise testing of your extracts and other substances.
 
endlessness
#2 Posted : 1/14/2010 2:07:15 PM

DMT-Nexus member

Moderator

Posts: 14191
Joined: 19-Feb-2008
Last visit: 16-Dec-2024
Location: Jungle
curious how it turns out Smile
 
soulfood
#3 Posted : 1/14/2010 2:12:24 PM

DMT-Nexus member

Senior Member | Skills: DMT, Harmaloids, Bufotenine, Mescaline, Trip advice

Posts: 4804
Joined: 08-Dec-2008
Last visit: 18-Aug-2023
Location: UK
Best of luck Smile
 
IAAGSOM
#4 Posted : 1/14/2010 2:36:42 PM

DMT-Nexus member


Posts: 98
Joined: 01-Nov-2009
Last visit: 16-Oct-2021
Ohoho, can't wait to hear results. Can't wait for my extraction to finish Very happy
.
 
Jorkest
#5 Posted : 1/14/2010 4:48:00 PM

DMT-Nexus member

Moderator | Skills: Extraction Troubleshooting, (S)elf ProgrammingChemical expert | Skills: Extraction Troubleshooting, (S)elf Programming

Posts: 4342
Joined: 02-Oct-2008
Last visit: 19-Jan-2024
yes please tell us how it goes!
it's a sound
 
LucidLemonade
#6 Posted : 1/14/2010 5:06:53 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
Will do... He just has to go out and take care of a few things first...

AS SWIM never toasted the seeds at any point he's guessing theres a slight chance this could be 5-meo-dmt if it is active at all.

SWIM might first take half of this extract and place in his volcano on MAX (260'c) and leave it in there for a few mins to hopefully vaporise off some of the lower temp actives, just to be sure.... & will then attempt to smoke between 5 - 15 mg & see how it goes...

Results later tonight....
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
soulfood
#7 Posted : 1/14/2010 6:47:56 PM

DMT-Nexus member

Senior Member | Skills: DMT, Harmaloids, Bufotenine, Mescaline, Trip advice

Posts: 4804
Joined: 08-Dec-2008
Last visit: 18-Aug-2023
Location: UK
Couldn't you just wash it thoroughly with naphtha?
 
LucidLemonade
#8 Posted : 1/14/2010 7:02:19 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
soulfood wrote:
Couldn't you just wash it thoroughly with naphtha?


Thats probably a better idea... but SWIM only has a small amount & no naphtha to hand at the moment....

He's also just started another 50g extraction, so will def pick up some napatha tomorrow & once he's got a larger amount to work with will try a napatha wash and see if that pulls anything else off.

Thnx.
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
LucidLemonade
#9 Posted : 1/14/2010 9:19:17 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
SWIM told me the following just happened...

First, SWIM can be a bit of a clumsy tit at times as he knocked over the 100mg of the ???? and only managed to recover about 15mg.....

This was about 1 hour ago.... smoked on top of a bowl of weed 5mg at a time...

Effects...

... Pins and needles thought-out whole body and especially in the head... very nice feeling... & feels like his head is expanding...

... Slight CEV...

... When opening eyes occasionally there's a very slight pause in being able to see... a bit weird...

... defiantly some euphoria, he still has a big grin on his face.. but that could be from just NOT throwing up.... usually happens with 5-ho-dmt experiments...

... Some OEV but very minor & they seem to disappear the second he notices them...

... Enhanced colours, very vibrant...

... NO NAUSEA!!!!! this is a first for SWIM he's thrown up many a time trying to work this out...


This is looking very promising....

Another batch of 50g seeds & 30gram Sodium-Carbonate paste is now drying...

More experiments to come tomorrow....

Smile
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
LucidLemonade
#10 Posted : 1/15/2010 6:03:18 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
A few quick pics of SWIMS second attempt...

1. 50g Cebil grinded up.
2. 25-30g of Sodium Carbonate & a little water added to make a paste.
3. Let dry over night.
4. Grind up again...
5. 3x 100ml of IPA added into a jar and shaken violently...
6. 300ml of IPA filtered 4 or 5 times.
7. 300ml of IPA split into 2.

8. 150ml of clean IPA & add about 1g of Furmic acid. a lot more than needed!
9. 150ml of IPA+Furmic added to 150ml of the IPA seed extract.
10. Loads of precipitation.
11. Pour off IPA carefully and the precipiation placed into glass baking try, placed on radiator to evoporate off the last little bit of IPA.

** Above 4 steps repeated with the other 150ml of IPA pulled from basified seeds...

SWIM is now guessing he has about 1g of a slightly off white/grey powder on the baking try...

Here are some pics under the microscope x400...

Later tonight SWIM will freebase and then pull again....

More results to follow.......

QUICK update: he maybe thinks this could just be Fumaric acid Crying or very sad Embarrased Crying or very sad just simply by the look of it...

He's told me he'll check tomorrow..... He really hopes not...Rolling eyes

LucidLemonade attached the following image(s):
1.jpg (425kb) downloaded 219 time(s).
2.jpg (418kb) downloaded 221 time(s).
3.jpg (423kb) downloaded 220 time(s).
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
Observant
#11 Posted : 1/16/2010 10:07:40 PM

Nothing Stops The Void


Posts: 739
Joined: 19-Jun-2008
Last visit: 26-Nov-2013
Location: Blinded by the Lye
Why should it be Fumaric Acid thats dropping out of the IPA ?
Had he more quickly realized just who they were,he would have shown them more respect.Had he tried harder to fathom their brilliant minds,he would have taken more of their teachings to heart.Had he more clearly understood the purpose of their being,
he would have more vigorously tried to assist them.They were truly honorable; he was sadly prejudiced.
They were exceedingly well informed; he was grossly ignorant.They were totally indefatigable; he so often, and so quickly,gave up. Still, for many years there was a strong inter-species alliance between the Eleven-Eleven of the Half-way Realm, their Seraphic Associates,and their flesh-and-blood friend, a common mortal. Much was accomplished, many profited, and, thereโ€™s only one regret...They could have achieved so much more...

All Hypnotizing Hypnotizes Hypnotizing
 
SpasticSpaz
#12 Posted : 1/16/2010 10:22:32 PM
DMT-Nexus member


Posts: 119
Joined: 02-Nov-2008
Last visit: 29-Jun-2011
SWIM's a big advocate of IPA for extracting bufo. He normally just does a crude basified IPA extract (which he sometimes blend with an equal amount of DMT and harmaloids, depending on mood), and he's never had undue nausea issues (He ALWAYS gets nauseous at first with bufo, even the one time he had beautiful off-white crystals, but it fades in minutes)
 
LucidLemonade
#13 Posted : 1/17/2010 11:28:32 AM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
Observant wrote:
Why should it be Fumaric Acid thats dropping out of the IPA ?


As it turned out it wasn't the fumaric acid and it did turn out to be the goodies... but was only about 400mg after it was scrapped up...

He then freebased it BUT got impatient waiting for it to dry & placed it in the oven & forgot about it, which pretty much destroyed most of it....

* he's noted from all his failed attempts that too much heat during the freebase drying stage seems to wreck it... def, let dry first before excessive heating....

At this point SWIM was a little upset....

He's paid his dues to the Buffo Gods so so so many times....

He's prayed at the white alter many a times after BAD failed attempts...

He's sarcified the contents of his stomach.... Solvents... Seeds... & more spare time than he cares to admit too....

"NOW, BUFO OWES HIM".....!

He's come so close...

But now he wants the goods...!

So he decided that this weekend, that it's payback...

He's gonna create a TEK that works....

And then it happened.... Smile

COMING very soon... To the greatest DMT & entheogen website in the known universe...

LucidLemonade Proudly presents... The....

Small scale... 10g Seeds to 100mg(ish) 5-HO-DMT TEK.....

It's only really a copy of other TEKS.... BUT it's the use of a few different bits of equipment makes the whole process easy, quick and painless & very efficient.....

Pics & TEK to follow later today..... Needs to first borrow a digital Camera to take a few pics to help explain it all.....


Sorry to be a tease................. Pleased


But I think it will be worth the wait....

Very happy
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
LucidLemonade
#14 Posted : 1/17/2010 11:30:36 AM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
Oooops... forgot to attach a quick pic of the goodies....!
LucidLemonade attached the following image(s):
PotOfGoldAtTheEndofTheRainbow.jpg (449kb) downloaded 168 time(s).
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
LucidLemonade
#15 Posted : 1/17/2010 1:37:37 PM

DMT-Nexus member


Posts: 124
Joined: 13-Aug-2009
Last visit: 13-Sep-2015
Location: Your are here <-----
SWIM has now scraped up a second batch that was drying from a glass baking tray... this is from first pull only, it looks so beautiful..... he believes theres still at least another 30mg in the second 25ml pull of Acetone....

Sorry, above should read... 5g seeds to 100mg 5-HO-DMT & only 100ml MAX of Acetone in about 1-2 hours......

Cool
LucidLemonade attached the following image(s):
PICT0307.JPG (85kb) downloaded 162 time(s).
"Let us declare nature to be legitimate. All plants should be declared legal, and all animals for that matter. The notion of illegal plants and animals is obnoxious and ridiculous" - TMK
 
ibeing897
#16 Posted : 1/17/2010 1:56:54 PM

DMT-Nexus member


Posts: 582
Joined: 10-Jul-2009
Last visit: 22-Jul-2014
SWIM is following this thread closely... good luck LucidLemonade... he is ready for another round of experimentation now he has more seeds, ISO, acetone, naptha and even some MEK to experiment with... wish I could find some heptane, I will maybe try some MEK:naptha ratios also.
all posts are fictional
 
jamie
#17 Posted : 1/17/2010 5:54:32 PM

DMT-Nexus member

Salvia divinorum expert | Skills: Plant growing, Ayahuasca brewing, Mushroom growingSenior Member | Skills: Plant growing, Ayahuasca brewing, Mushroom growing

Posts: 12340
Joined: 12-Nov-2008
Last visit: 02-Apr-2023
Location: pacific
"5g seeds to 100mg 5-HO-DMT & only 100ml MAX of Acetone in about 1-2 hours......"

Yeah that sounds about right..from 6 grams of my seeds extracted with iso I get 10-12 very strong visionary doses..I think 8-10 mg is a good dose that should blow you away into deep visions every time.

Long live the unwoke.
 
Observant
#18 Posted : 1/17/2010 8:26:27 PM

Nothing Stops The Void


Posts: 739
Joined: 19-Jun-2008
Last visit: 26-Nov-2013
Location: Blinded by the Lye
The Ipa / FASI approach seems to be giving me great results .

It also gave me some off white precipitation from freebased mesc acetate resins .
Hopefully Mescaline Fumarate
Had he more quickly realized just who they were,he would have shown them more respect.Had he tried harder to fathom their brilliant minds,he would have taken more of their teachings to heart.Had he more clearly understood the purpose of their being,
he would have more vigorously tried to assist them.They were truly honorable; he was sadly prejudiced.
They were exceedingly well informed; he was grossly ignorant.They were totally indefatigable; he so often, and so quickly,gave up. Still, for many years there was a strong inter-species alliance between the Eleven-Eleven of the Half-way Realm, their Seraphic Associates,and their flesh-and-blood friend, a common mortal. Much was accomplished, many profited, and, thereโ€™s only one regret...They could have achieved so much more...

All Hypnotizing Hypnotizes Hypnotizing
 
69ron
#19 Posted : 1/17/2010 8:41:48 PM

DMT-Nexus member


Posts: 5826
Joined: 09-Jun-2008
Last visit: 08-Sep-2010
Location: USA
Observant wrote:
The Ipa / FASI approach seems to be giving me great results .

It also gave me some off white precipitation from freebased mesc acetate resins .
Hopefully Mescaline Fumarate


Observant, can you go into more detail about this in one of the mescaline threads? I would love to hear more about it.

SWIM tried making mescaline fumarate precipitate from d-limonene. He saturated acetone with fumaric acid, added it to the d-limoenne with the freebase mescaline in it, and all that happened was fumaric acid precipitated out. No mescaline ever did. It was disappointing.
You may remember me as 69Ron. I was suspended years ago for selling bunk products under false pretenses. I try to sneak back from time to time under different names, but unfortunately, the moderators of the DMT-Nexus are infinitely smarter than I am.

If you see me at the waterpark, please say hello. I'll be the delusional 50 something in the American flag Speedo, oiling up his monster guns while responding to imaginary requests for selfies from invisible teenage girls.
 
damiana
#20 Posted : 1/17/2010 9:03:47 PM

Cosmic Dragon


Posts: 460
Joined: 25-Feb-2009
Last visit: 16-Jul-2014
Location: Chi Town
Looking forward to this tek with pictures, hurray. Smile
PEACE
 
123NEXT
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.036 seconds.