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Distilling limonene? Options
 
PlainCoil
#1 Posted : 9/29/2009 12:42:04 AM

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Cactus is cheap. Pickling lime is cheap. Water, vinegar and carbonated water are all dirt cheap. The only thing that hurt's SWIM's wallet is d-limonene.

SWIM read in another thread about distilling used limonene easily, and SWIM would love to know how. He's never distilled anything before...

Any help would be appreciated.... by SWIM.

thanks

 

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MagikVenom
#2 Posted : 9/29/2009 1:49:58 AM

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Any good organic chemistry book that goes over standard lab practices should give the procedure for distillation. The difficult expensive part will be constructing the apparatus. It can be a bit dangerous ie still explosion so do lots of research and make sure you completely understand the distillation process and follow all safety practices to a T. Not sure about distilling orange oil never looked into that.

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MV

 
benzyme
#3 Posted : 9/29/2009 4:47:27 AM

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limonene distills at 176C, i think.
(go with all glass setup, plastics and rubber may soften/warp)
under reduced pressure, you could distill it at a much lower temp (vac. distillation).


steam distilling limonene involves simple distillation of water with ground orange and lemon peels.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
 
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