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water in field. how to rescure? Options
 
Gardenic
#1 Posted : 6/21/2015 9:34:37 PM
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Hello, i just took (very carefully) pyrex from freezer,

First thing I noticed were loose crystals "swimming" in a dish.

after 15 minutes, field still dont want to dry. i decide to scrape all field, now i have wet mass.

I think water could somehow get from the freezer to dish, I left it open for a while by accident.

Can i rescue this somehow?

it is almost end of my mimosa, which is very very difficult to get in my country;/ (cost two monthly salary) I would like to not lose the last milligrams of my dmtSad
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STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
Tryptallmine
#2 Posted : 6/21/2015 11:09:44 PM

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Gardenic wrote:
Hello, i just took (very carefully) pyrex from freezer,

First thing I noticed were loose crystals "swimming" in a dish.

after 15 minutes, field still dont want to dry. i decide to scrape all field, now i have wet mass.

I think water could somehow get from the freezer to dish, I left it open for a while by accident.

Can i rescue this somehow?

it is almost end of my mimosa, which is very very difficult to get in my country;/ (cost two monthly salary) I would like to not lose the last milligrams of my dmtSad


Take it out of the freezer, let it all melt. Add 50ml of warm/hot solvent and mix it around. If you can put the whole thing in a mild heat bath then do that. It'll make sure all the DMT that has formed on the layers of the crystallizing dish dissolves back into the solvent.

Decant this into a 100ml beaker or tall thin glass (large shot glass?) so it's easier to work with.

The water will end up at the bottom of the glass, remove it with a pipette or syringe to the best of your abilities. Get it all out, even if it means losing a few ml of naphtha.

Put the solvent back in your (clean) crystallizing dish and evaporate a little bit of the solvent until you see it saturated again.

Seal it up properly, put it back in the freezer and don't touch it for 24 hours! Problem solved Smile
 
LSDvibes
#3 Posted : 6/22/2015 12:41:37 AM

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Wish I had come across this thread earlier when I was having the same problem, great advice and good luck, gardenic!
 
Gardenic
#4 Posted : 6/22/2015 12:46:51 AM
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Thanks Tryptallmine, and LSDvibes!
i hope this will workRazz


This is how my dmt looks like,
realy realy bad



after flushing was a lot of fat..



it's a very surprising, because it is always little more or little less like this.




I will share a pic in 24h, when dmt will freezing after recrystallizationSmile
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Gardenic
#5 Posted : 6/23/2015 1:45:46 PM
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successSmile
i recrystalizing all what i got, but.. from 1g i ave now somethig about 200mg;p

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LSDvibes
#6 Posted : 6/23/2015 3:58:37 PM

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Gardenic wrote:
successSmile
i recrystalizing all what i got, but.. from 1g i ave now somethig about 200mg;p


That yield loss seems high but maybe there were a bunch of fats/oils that got into the mix? But great work! Your DMT looks nice and fluffy!
 
Gardenic
#7 Posted : 6/23/2015 4:04:24 PM
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i think, after recrystallization, in a glass was something about 5ml of fat.

I recrystalized this "wet part" and some good part (didnt taking picture), good part is something about 3 times more, than after recrys;p but any way, its good, now i have pure pure dmt;p
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