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Add hot xylene to cold or hot base solution? Options
 
damiana
#1 Posted : 3/9/2009 11:42:09 PM

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Does anyone know if a higher yield results from adding hot xylene(or any non polar solvent) to a cooler or hotter MHRB base solution? Thanks.
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benzyme
#2 Posted : 3/10/2009 12:00:52 AM

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hot xylene --> room temp basic solution.

heating the base isn't a good idea; once dmt is in free-base form, it becomes more volatile. even simmering basic solution may cause dmt to evap from the solution
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