Quote:did the tek as stated got a lot of clear oil with dmt crystal sitting on top of it
Which tek? How many pulls so far? 5 isn't unheard of...
Is the clear oil after evap of hexane? Or? Any oily/fatty/waxy stuff likely has goodies - do a re-crystallization with a small volume of NP solvent.
BTW, mind resizing the pics? And perhaps including one of the original bark?
Quote:why would it all just crash out??
Perhaps the solvent is quite saturated - have patience with a COLD freeze and I suspect you will be pleased.
Don't throw anything away. Let us know.
Best, L
"The first principle is that you must not fool yourself, and you are the easiest person to fool." Richard P. Feynman