So, after swims nice and leisurely a/b using d-limo and fasw/fasi/and a little fasa to salt his alkaloids he was left with a crumbly, bitter, yellow powder. Each salting method was used on different pulls, not combined in one salting. He knew it was not pure n,n dmt fumarate, and most definitely had some other alkaloids and possibly fats and or oils.
Swim collected approx 2+ grams of jimjam fumarates from his two 100g extractions. He had no prob. using the product as-is for pharma, and even fb'ed some and made changa with anhydrous iso. Worked fine, well rather well for pharma, and so-so for vaporizing. Swim thinks its either oxidized, or the iso pulls some impurities as well. Anyway, swim recently got a hold of some anhydrous acetone. He had heard lots of reports of people washing excess fumaric acid from their pulls, usually because fasa pulls less other alkaloids and more nn. However, swims jimjam fumarates were precipitated or salted from his limo with multiple solvents, and probably contributed to its full-spectrumness.
So swim decided one day to wash his remaining fumarates with acetone, partly bec. swim is doing another extraction on 500g mhrb and will have more spice to work with. He wanted to test this on this spice so he can use it in that tek. 1.130g of jimjam-fumarates were washed with anhydrous acetone. Swim pulled until the acetone took on a clear color v. yellow. He was left with approx 750mg of pinkish fumarates that looked much nicer than before, and had none of the waxiness displayed previously. He evapped the acetone and was left with an orange/yellowish crumbly powder.
Swim is wondering, does anyone have any info as to what was separated? IE- have you experienced anything like this washing fumarates with acetone? Also, hes sure that there's something active in the orange wax. Hoverer, it would have to be jungle, or n-oxide or something else.
Any comments or information/links are welcome.
Thanks-
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