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Lifting_the_veil
#1 Posted : 1/23/2011 10:42:58 PM

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with mimosa extraction going STB, What is the yield comparison using glass jars with moderately warm water that is barely agitated (slight roll, or doorknob shake) VS. a milk jug that you have to shake vigorously for the reaction?

On the latter pulls will it yield more if heated to 120 for 20 minutes before separating?


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soulfood
#2 Posted : 1/23/2011 11:36:28 PM

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They will both yield the same as long as you persist until you stop yielding.

TADA!!!

Obviously though more vigorous agitation will be more effective.
 
Ljosalfar
#3 Posted : 1/24/2011 12:30:17 AM

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To avoid very inconvenient emulsions, be sure SWIY's pH is 12+... an excess of NaOH will accomplish this, and then it is safe to shake vigorously.
Warming the extraction seems to make it a bit more efficient. Like Soulfood says, pull till it's spent... then look into pulling with a different solvent (Xylene, for example), and salting out the last of the last!
Bon voyage!
L
"The first principle is that you must not fool yourself, and you are the easiest person to fool." Richard P. Feynman
 
 
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