TL/DR: 15min tek for clear to white spice.
fresh from the lab!

Materials:
100g pre powdered MHRB
100g Lye crystal
600ml distilled water
75ml of bestine brand or similar pure heptane.
long pipette of syringe with tube attached.
750ml alcohol bottle or similar glass seal-able vessel.

1. over the course of 10min add lye to water in the bottle. shake and stir very well. be sure to vent from time to time. i run it under a gently cool water sink just in case. but you CANNOT let it get cold. once all 100g have dissolved and the water has cleared from it's cloudy state move to step 2.

2. using a funnel add 100g of mhrb. shake bottle to mix. when shaking in this step and the prior remember that hot liquid in a closed bottle causes the air inside to expand. avoid spraying your hands with basic liquid when unscrewing cap. the bottle should be warm to hot at this point. just avoid simmering the water.

3. immediately add the 75ml of heptane and shake like mad. heptane does not dissolve dmt well when anything but boiling. if you have done steps 1 and 2 correct the heat from the basic root mixture is enough to do this.

4. let the bottle settle for 5 or so min. i place my bottles on the subwoofer of my computer. 2min of dubstep is enough to break any emulsion ive seen yet. it also makes the solvent separate much much faster. heptane also seems to split faster than naphtha with a normal stb.

5. at this point the heptane should be on top and not have any black gew floating in it. it may appear cloudy or bubbly or something of the sort. this is(should be) the heptane boiling. but you deff dont want any bubbles of dark liquid. using your suction device remove most of the heptane. i can get about 65-70ml of the initial 75ml before it is too annoying to continue. never risk the purity of your 70ml of pure solvent for that last 5ml. we shall see it again anyway ;]

5.5 the second you suck the heptane into your pipette it should become VERY cloudy. almost totally opaque. this is the deadman's test to see if you ran this tek correct. the heptane should been hot enough in the bottle to dissolve huge amount of dmt, but as soon as it hits the pipette it will cool enough that the dmt will begin to fall out of solution causing the color shift.


6. place the solvent in a lidded non reactive jar and place in the freezer. in my experience due to the saturation of suddenly non soluble dmt, just 3min in the frz and you can see crystals growing(not just precipitating but growing like real crystals should). after one night in the coooooold freezer(cold enough that my veggies freeze in the fridge!)

7.pour the heptane into a beaker taking care to pour slow enough to not wash all free floating crystals out. most all your dmt should be stuck to the jar pretty good. not like a naphtha FP, but actually caked on and stuck to the jar. you can now pour this cleanish heptane back into your bottle of basic liquid.

I am able to do this start to finish in 15min plus the night in the freezer. it yields pure clear to white to slightly off white crystals. most of which stay separate in the jar so if you take care scraping you can keep them apart.

this tek depends on a few key things.

-saving the heat energy from the basification to boil your naptha.
-pre powdered mhrb does not need more than 5min in solution to break down the cellulose and free the dmt.
-using heptane.
-woofer helps seperate while remaining HOT!

for your second pull i suggest capping your bottle with the base liquid and heptane and running it under a sink for 20min. most household sinks will hit 180 or atleast 140 which is enough to boil the heptane. i do not know the effects of letting the heptane soak in the bottle for more than a couple min. contam may go up.

after 2 or 3 pulls i switch to naphtha and do your normal normans tek to pull spice. a combo of cooling pulls durring FP will ensure no oils. to do this siphon off the solvent after 10-20min in the frzr. place the yellow solvent in a clean jar and continue the FP. once the orange/brown goop has fallen out but not the dmt. this yields a crystalline/fluffy yellow spice. if you dry the goop you get orange spice.

i save my goop in a jar and am growing red crystals in brown oils atm.

No real innovation here beside the sujbwoofer thing to break emulsions, pretty creative

Despite only having slight variations from my current technique, I might try elements of this to improve my results.

Thank you very much for taking the time to help =)

oh believe me i know there is nothing new here. its just imo a great way to make your first pull from a batch of mhrb and get white dmt in 20min. beats doing 5 naphtha pulls and 3 days of rexing etc. this way you get most all of your white dmt on the first pull, then you are free to do what you want to get the jungle.

also using the heat from the lye eliminates a whole step of boiling and extra jars and a big water bath for your jug etc.

basically i was able to do this in 1/3rd the time in my bedroom vs out in the kitchen.

important also is that there is zero need to let the cellulose decompose. at least for that first night every tek says to do. im just really tryign to say how awesome heptane is! haha.

also, heptane seems to allow for actual crystal formation muuuch better than naptha.or atleast its volitility speeds it up.

Haha, what an ingenious idea! I will for sure try that next time - can't believe I haven't thought of it. Thanks for sharing your tek.

i must give credit where it is due. a member here posted something about setting their jug on their motorcycle with the choke on. that reminded me of using a vibrator in a lab. when i was 16 i had a bio lab where we did the dna electrolysis thing and one step was to use these hotplate looking things that vibrated like mad. i happened to be listening to some dubstep while mixing some base/naphtha last week and just set it on there. was perfect.


ty

Tangarine_Dreams wrote:



that was g1r, I believe.

JBArk

Nice experimentation

Whats the yield on the first pull, seems like it would likely but much lower than a pull that would be done after a day since STB teks tend to take a while.

SWIM can do his lime/vinegar tek and get .5-.75% white spice in 45min-60min but there is no need to rush spice...

He never got above .1% when he did STB with lye even on the first pull after leaving for 1-2 hours and got the majority after 2 days.

i can easily pull 1g of dmt with 100ml of room temp heptane...no problem

i dont have a digi, only a triple beam good for weighing components. but i use these tiny glass vials from the hobby store to keep it and the first pull filled 3. my last batch of 100g filled about 6 after doing 6-8 pulls with naphtha.

tho this may also mean nothing cause the white may be much more voluminous.

see if i leave my naphtha in for 5min and remove it i dont get much dmt but it is light yellow. if i soak naphtha over night i get very orange solvent when i pull. i have not tried leaving heptane in over night but id say i only got 4mg of dmt in a 5min pull with vm&p vs >300mg with the hot heptane

What are the vials meant for? I had a vial from lab I was using but someone walked off with it and I have a new batch that needs storing. Where in the hobby store do they sell little DMT vials?

well for one its a lady oriented hobby store. like. fake flowers arts furniture decorations etc. the manly hobby store yielded nothing good and the ppl running it were much more pressing to knwo what you were working on lol. tye dye is a very similar application in chemical needs. sept the heptane.

g5arden r5idge, hobb5y lobb5y, rarely michae5ls. 5's are to not bring that up on google.

the vials are in the bead isle. with the odd silver and metal bits. treasure something i think is the name. there are long thin ones, like 1" tall and 1/4th in wide. little rb flask ones that are cute and hold alot. and little jars that are about .75"in by 3/8ths. 2 of each kind for 1.47

bestine is 4 isles over in the drafting supply isle. in the one owned by mornon's anyway.

PEOPLE LISTEN TO ME!!!!! MWAHAHAHHAHAHAH!

Nice!!!
All sounds pretty good, will try this in the next few weeks.

Especially liking the subwoofer part - dubstep bass is the energy needed for SURE.

This tek looks interesting, the tek swim does @ the moment is very similar to this

And have wanted to use heptane in a extraction for a little while