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does sodium carbonate wash = loss of N oxide and jungle Options
 
Jin
#1 Posted : 2/19/2010 5:10:40 PM

yes


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i am doing a STB on MHRB using toluene as my non polar solvent , so giving it a non polar wash with sodium carbonate before evaporating.
will this result in the loss of N oxide and jungle ? as i want these in my spice
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amor_fati
#2 Posted : 2/19/2010 5:32:52 PM

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Jin wrote:
i am doing a STB on MHRB using toluene as my non polar solvent , so giving it a non polar wash with sodium carbonate before evaporating.
will this result in the loss of N oxide and jungle ? as i want these in my spice


SWIM's fairly sure there shouldn't be N-Oxides in there at all. The jungle should remain. SWIM's never really known anyone to do a wash on toluene or xylene, as usually used to get a whiter product with naphtha. Evaping toluene is a fairly nasty route. The preferable manner of using xylene or toluene is with the FASA method.
 
mumbles
#3 Posted : 2/20/2010 6:32:25 AM

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It shouldn't, because as the freebase they should be insoluble in basic water. Evaporating off toluene or any other solvent will leave you with a heap of shit. Do FASA, a freeze precip, anything but leaving the shit to dry to an oily contaminated mess.
 
 
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