Anyone ever encounter this?
After soxhlet pull, egg wash, 2 salt precips a ton of nice big crystals were left. Didnt weigh but about 3/4 inch up a 1000ml beaker. It was re-disolved in hcl water (700ml) and filtered (like every other salt precip) this time 1/4 tsp of activated choracoal was poured in and put on stir plate for 5 minutes. It was then filtered and saturated with salt.
This time though, there is about 1/4 inch of precips but the liquid if full of crystal shards in suspension....
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