We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Room temperature Bestine Recrystalization Options
 
futura
#1 Posted : 12/7/2009 6:28:56 AM

DMT-Nexus member


Posts: 86
Joined: 27-Oct-2009
Last visit: 04-Dec-2017
I used the marsofold a/b tek on 1 KG Mimosa Powdered Pink Inner Root bark.
I went with a PH of 4(Distilled Water/White Vinegar) on the A step(1 Gallon-3to1 Ratio-Water/Vinegar per 500g)
and a PH of 13.4(Distilled Water+Lye -(1 Pint Water+70 G Lye)on the B step
Three Crock Pot simmers for 2 hours each stirred every 15 minutes
Decanted and vacum filtered all particles out before adding Lye
I extracted 3 times Using Lab grade Pet Ether for the Extractions(500 ML Each Extraction)
Reduced it to 20 % of original volume and Freeze precipitated
I kept each extraction seperate
First extraction resulted in off white xtals 7.5g
Second resulted in slightly yellow xtals 1.0g
third resulted in yellower X-tals .5g

I will do re-xtailization on each pull seperately...

I have found some help here on this outstanding forum in this post as follows...

http://www.dmt-nexus.me/....aspx?g=posts&t=1266

Can anyone suggest some other links on recrystalization??

Thanks!!!!!
 

STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
cashewman1
#2 Posted : 12/7/2009 9:55:05 PM

DMT-Nexus member


Posts: 38
Joined: 03-Nov-2009
Last visit: 26-Feb-2010
Location: Between the S and P orbitals
http://www.dmt-nexus.me/....aspx?g=posts&t=4705

Recrystal vid in there somewhere, should help
I am here to restructure my priorities in a way to most benefit all

-Everything posted here is fantasy please do not misinterpret the posting of a role playing board for reality
 
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.008 seconds.