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dark naphtha problem - what solution works for you? Options
 
jiva
#1 Posted : 11/11/2018 7:43:48 PM

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Last visit: 07-Sep-2022
hi everyone,

so i am having dark naphtha issues again. so far whenever i've had this issue i did a mini A/B and eveything was fine.
online i found other approaches like doing a re-x.
then i found one site where someone wrote they don't do anything, just let the naphtha sit at room temperature for a few hours. apparently it the particles tend to separate out over time.

what i did just now is transfer the naphtha into a new narrow bottle with a bit of water and sodium hydroxide at ph 14.
i am curious how clean of a product this method can produce.

have you got any other solutions for this issue?
 

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skoobysnax
#2 Posted : 11/13/2018 2:47:41 PM

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jiva wrote:
hi everyone,

so i am having dark naphtha issues again. so far whenever i've had this issue i did a mini A/B and eveything was fine.
online i found other approaches like doing a re-x.
then i found one site where someone wrote they don't do anything, just let the naphtha sit at room temperature for a few hours. apparently it the particles tend to separate out over time.

what i did just now is transfer the naphtha into a new narrow bottle with a bit of water and sodium hydroxide at ph 14.
i am curious how clean of a product this method can produce.

have you got any other solutions for this issue?

Try a sodium carb wash of the Solvent. Be sure there is enough solvent to keep the alks from dropping out at room temp.
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jiva
#3 Posted : 11/13/2018 11:01:45 PM

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Posts: 421
Joined: 14-May-2016
Last visit: 07-Sep-2022
i just let it sit for a night
pulled it out of the freezer today, i got very nice crystals, but with a little goo at the bottom, that had a brownish color when scraped up.

i will re-x and i think it will be a nice result
 
 
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