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Red oily precipitate from spent naphtha? Options
 
Jagube
#1 Posted : 7/20/2018 2:33:31 PM

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After freeze-precipitating my last pull with naphtha, I saved the solvent in a jar for re-use in the next extraction.

I forgot about it and when I found it weeks later, there was a red / reddish orange precipitate at the bottom of the jar.

Any idea what it is? Could it be the jungle alkaloids, which the naphtha pulled, but the freeze precipitation didn't retrieve?
Jagube attached the following image(s):
red oil.jpg (625kb) downloaded 67 time(s).
 

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Silly(c)One
#2 Posted : 8/5/2018 7:18:23 PM

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It looks like DMT-N-Oxyde to me, but I'm no expert Razz
 
 
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