Jagube wrote:Do you pour off your naphtha and evaporate the remaining bits and the crystals still remain solid and only melt upon scraping? Or do they melt already during the evaporation?
Yes, the above photo was taken after I poured off the naptha into another glass container (the excess naptha is tinted yellow btw), and put the pyrex container back into the freezer with lid on, upside down to allow any excess naptha to drip off.
Now every time I attempt to scrape off the goo/xtals they melt back to liquid instantly on contact.
I just re-read some posts and realise I might have missed something. After freeze precipitation, it seems I should still do air evaporation? I previous thought it was either/or, but it seems I need to do both?
Jagube wrote:Are you sure those crystals are DMT indeed?
The container certainly smells like DMT. What else could it be? Is it possible that something other than DMT was extracted and forms goo/xtals?
Jagube wrote:I've had naphtha pulls from A. floribunda and P. aquatica melt during evaporation.
For the future, a defat of the acidic brew might help. Another solution (if it's DMT indeed) would be to use limonene as the NPS and backsalt it. Then re-base, pull with IPA or acetone and evaporate that.
This is my first extraction, and such did a straight A/B extraction, I didn't really want to over complicate it, but maybe on my next attempt (I still have about 200g of floribunda phylodes left) I'll read up on defatting.