DMT-Nexus member
Posts: 144 Joined: 24-Mar-2018 Last visit: 19-Aug-2018 Location: New york
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When salting dmt does any nmt in with it also turn into a fumerate?
You are an explorer, and you represent our species, and the greatest good you can do is to bring back a new idea, because our world is endangered by the absence of good ideas. Our world is in crisis because of the absence of consciousness.”
-Terence McKenna
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DMT-Nexus member
Posts: 144 Joined: 24-Mar-2018 Last visit: 19-Aug-2018 Location: New york
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Just searching for separation techniques. Seems dry ice is the way to go.
You are an explorer, and you represent our species, and the greatest good you can do is to bring back a new idea, because our world is endangered by the absence of good ideas. Our world is in crisis because of the absence of consciousness.”
-Terence McKenna
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DMT-Nexus member
Posts: 307 Joined: 11-Oct-2015 Last visit: 30-Nov-2022
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I've heard that should work, not sure though.
Sometimes if I saturate hot naphtha and leave it in a cupboard the dmt falls out at room temp leaving the gooeys behind for a freeze pecip or evap.
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DMT-Nexus member
Posts: 183 Joined: 10-Jun-2017 Last visit: 13-Jul-2020
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Yes, nmt would form a fumerate, giving you a mixture.
The simplest method of separation is fractional crystallisation, as kloudQ7 has suggested.
This doesn't always work though as the solubility of nmt in aliphatic hydrocarbons is poorer than dmt, meaning that nmt should drop out of solution first.
If you are looking for a chemical means of separation, then two methods have been discussed here,
Acetylation with aspirin or carbamic acid formation with carbon dioxide.
Acetylation is more likely to be successful, I suspect.
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DMT-Nexus member
Posts: 307 Joined: 11-Oct-2015 Last visit: 30-Nov-2022
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Yes, the fractional crystallization usually only works that way for me when the bark contains more dmt than nmt then the crystals come out first. Slow cooling is the key.
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