Not that this is any different then the other STB extracts but i fdeel that be for i went into this i could never get a full grasp on this its practically like taking candy from a baby REALLY good candy
so anyway i just wanna lay this out so as to possibly help someone elce i have recomendations thru my trial and error
Things you will need according to me ..NO Plastic.. Im no chemist but NaOH n plastic just seems like a bad idea
So anyway:
#1.A thick glassed vase
#2.A pan that u can set the vase in about half the size
#3.A metal stirring stick
#4.A pyrex dish 4x4 5x5 6x6
#5.A glass pipette
#6.A roll of plastic wrap
#7.Sodium Hydroxide (NaOH)
#8.VM&P-Naphtha
#9.Your choice of bark (ACRB-MHRB)
#10.Distilled Water (H2O)
#11.A glass Measuring Cup (ML measurements)
(#12.Your time and patience)
Okay Process Time:
Fill your pan 3/4 the way with hot water
Place on electric stove on low (shouldn't come to a boil)
Get your vase and add (IN THIS ORDER)
1) 750ml Distilled water
2) 50g of NaOH (Add slowly while stirring AVOID skin eyes!)
3) 50g of Bark
Ok now once you've thoroughly mixed your solution for 5-10 min set your vase in your pan on the stove
So now let that set on your stove for 1-2hr while the NaOH dose its job and be sure to stir your emulsion every 10-15 min.
(Repeat this step 3x)-Next use a glass measuring cup with ML measurements on it and measure 50ml of Naphtha add that to your emulsion
Stir it in well, stir it about every 5 min for about 15-30 min allow time for the solution to settle out the clear layer on the top will now have the desired alkaloid in it
Use your pipette and gently suck up the clear layer and dispense it into your glass pyrex dish
Add another 50 ml of Naphtha and repeat for the 2nd time pull then repeat for the 3rd time
Now that you have all your solvent in your Pyrex dish cover it with plastic wrap and put it in the freezer for 24 hrs do not disturbing your dish
Yay your all exited now to have returned to your freezer to see the white crystals but your not quite their yet so at this point what u need to do is get a mason jar and use your pipette and suck off as much Naphtha as you can and store it in the mason jar into the freezer for re-use
Set your dish upright about 2 ft from a fan on high and wait about an hour it is now time to (Lightly Scrape) your crystals their is a oily sticky layer in the dish below the crystals. Collect all the crystals from top the sticky layer by using a razor
RE-Crystallization step:
Once collected and in a separate container return to your dish and scrap as much as u can into a shot glass. Using roughly 25-50 ml of warm naphtha (WARM NAPHTHA IN WATER BATH ONLY)
Add the naphtha to your dish and swish it around tilt the dish to a corner and suck up the naphtha and dispense it into your shot glass them cover and put in freezer for 12-24 hr (best to use clean naphtha for Re-crystallization
Im growing weary of typing at this point thats the cut and dry aspect i will further revise in the morning I plan on adding pictures PM me if you have questions