So you are on the final basing step, correct? The harmalas crash out during this step but if too much sodium carb is added, you will have excess in the final product.
So yes, I would let your mix sit overnight at least.
Tomorrow, most of it should have settled, if not it isn't a big deal.
Filter through a coffee filter.
Keep solids.
Discard liquids (check pH of water first).
Now, to get rid of excess sodium carbonate you need to do a water wash or two. This means adding water to your freebase harmalas. Filter through coffee filter. Keep solids. Discard liquid (check pH of liquid). You want the pH to be around 8 before it is generally accepted as "pretty pure" ...
After that you should be all set. Hope that helps, xa!
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