Come what may
Posts: 1698 Joined: 08-Mar-2015 Last visit: 23-Mar-2019
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Jees wrote:benzyme wrote:one could easily manage without a sep funnel. add a lighter-than-water solvent that dmt is very soluble in, but won't freeze (like ether or toluene) and decant... Bonus: one gets the best possible separations no matter how hard and long was shaken. Some lab-equipment of my interest in on this picture: Yeah....nice beakers! "In the universe there is an immeasurable, indescribable force which shamans call intent, and absolutely everything that exists in the entire cosmos is attached to intent by a connecting link." ~Carlos Castaneda
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Music is alive and in your soul. It can move you. It can carry you. It can make you cry! Make you laugh. Most importantly, it makes you feel! What is more important than that?
Posts: 2562 Joined: 02-May-2015 Last visit: 04-Sep-2023 Location: Lost In A Dream
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I would like to try out a separatory funnel (as some others have said) just to see if it was really more efficient. As of now, I just use a glass turkey baster. With practice it is easily mastered. I would also like to get a nice set of beakers! I've taken apart a couple of 1L french presses because they are essentially a beaker with some extra parts! They are perfect for 100g extractions! However having a set of professional beakers would have its advantages, I'm sure! New to The Nexus? Check These Out: One Fish Two Fish Red Fish Blue Fish
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analytical chemist
Posts: 7463 Joined: 21-May-2008 Last visit: 14-Jan-2025 Location: the lab
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DmnStr8 wrote:benzyme wrote:Misonix S-4000, 1" probe. one could easily manage without a Misonix S-4000, 1" probe. think outside the box... indeed but try lysing as thoroughly and quickly (including a PC) with anything in the kitchen, garage, etc. nothing else comes close. i suppose the sep funnel is just as good with instant gratification, it was my first piece of glassware i also suppose the thread is about what your priorities are. "Nothing is true, everything is permitted." ~ hassan i sabbah "Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
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DMT-Nexus member
Posts: 399 Joined: 21-Feb-2015 Last visit: 18-Feb-2018 Location: here
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I have a 500ml sep funnel, but i'm new to this thing and use only tek with the plant material left inside so i can't use it, but for mini a/b or wash my pulls with distilled water works great. Maybe the next time i try a tek with acid boils and filtration... Only one thing with sep funnel, what do you use for lubrificate the valve ? i try with vaseline but after a few separation the valve block and i have to clean and restart...what i can use that acid, base and naphta dosen't wash away ? >>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>> 0 <<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<
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analytical chemist
Posts: 7463 Joined: 21-May-2008 Last visit: 14-Jan-2025 Location: the lab
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silicone grease. or a round of ptfe tape. "Nothing is true, everything is permitted." ~ hassan i sabbah "Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
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xͭ͆͝͏̮͔̜t̟̬̦̣̟͉͈̞̝ͣͫ͞,̡̼̭̘̙̜ͧ̆̀̔ͮ́ͯͯt̢̘̬͓͕̬́ͪ̽́s̢̜̠̬̘͖̠͕ͫ͗̾͋͒̃͛̚͞ͅ
Posts: 1716 Joined: 23-Apr-2012 Last visit: 23-Jan-2017
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Is this an acid lab assistant or am I hallucinating the swirls and sparkles? And why is this from dreamstime.com? Where dreams come true or what?
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DMT-Nexus member
Posts: 399 Joined: 21-Feb-2015 Last visit: 18-Feb-2018 Location: here
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benzyme wrote:silicone grease. or a round of ptfe tape. thanks, ptfe tape, the one used by plumbers to seal joints pipes..good....i try it :-) >>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>>> 0 <<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<<
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DMT-Nexus member
Posts: 3574 Joined: 18-Apr-2012 Last visit: 05-Feb-2024
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Please do not PM tek related questions Reserve the right to change your mind at any given moment.
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DMT-Nexus member
Posts: 614 Joined: 02-Aug-2014 Last visit: 14-Sep-2024
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Nibbana
Posts: 15 Joined: 07-Dec-2014 Last visit: 09-Aug-2018 Location: Down under
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Definitely a good quality 1 or 2L borosilicate glass bottle with a screw cap. ^^ Comes in handy for all teks.
Would have said the glass syringe tbh but I haven't found a good household substitute for a good glass extraction vessel.
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DMT-Nexus member
Posts: 100 Joined: 14-Feb-2015 Last visit: 20-Dec-2017 Location: Everywhere and nowhere at the same time
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IME I would have to go with a 50ml glass syringe but I also love having a 2000ml volumetric flask... having the right equipment for the job makes a huge difference so It's difficult to pick just one but the glass syringe is on the top of my list All things stated within this website by myself are expressly intended for entertainment purposes only.
All people in general, and users of this site are encouraged by myself, other members, and DMT-Nexus, to know and abide by the laws of the jurisdiction in which they are situated.
I, other members, and DMT-Nexus, do not condone or encourage the use, supply, or production of illegal drugs or controlled substances in any way whatsoever
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DMT-Nexus member
Posts: 614 Joined: 02-Aug-2014 Last visit: 14-Sep-2024
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Damn with those syringes. I have 20 ml one, and believe me, pipette rules! It is so easy to suck in bits of basic soup with glass syringe. Glass syringes are not smooth as plastic ones.
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DMT-Nexus member
Posts: 100 Joined: 14-Feb-2015 Last visit: 20-Dec-2017 Location: Everywhere and nowhere at the same time
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oversoul1919 wrote:Damn with those syringes. I have 20 ml one, and believe me, pipette rules! It is so easy to suck in bits of basic soup with glass syringe. Glass syringes are not smooth as plastic ones. My 50ml is super smooth and so far it has worked flawlessly for me but I have been seeing a lot of people express how much more efficient pipettes are so that will probably be my next piece of equipment to try... I was thinking glass 10ml with a hand pump most likely. Another one I have been trying to track down is the conical measure gibran pictures in his caapi extraction tek... I have been using a small conical vase which has worked fine but I'm always looking to upgrade All things stated within this website by myself are expressly intended for entertainment purposes only.
All people in general, and users of this site are encouraged by myself, other members, and DMT-Nexus, to know and abide by the laws of the jurisdiction in which they are situated.
I, other members, and DMT-Nexus, do not condone or encourage the use, supply, or production of illegal drugs or controlled substances in any way whatsoever
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Communications-Security Analyst
Posts: 1280 Joined: 17-Aug-2014 Last visit: 05-Feb-2024 Location: Nirvana
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My glass syringes are fitted perfectly, stainless steel luer lock tips/dispensers. Pipettes ftl.
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DMT-Nexus member
Posts: 874 Joined: 24-May-2014 Last visit: 22-Jun-2024
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I have 20/50/100 ml Glass syringes . Prior to those I used plastic ones which after a few used would stick , I even used to oil the edge of the plunger as I went and I received blisters on my hands to boot. Glass syringes are the dogs nuts in my books
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DMT-Nexus member
Posts: 614 Joined: 02-Aug-2014 Last visit: 14-Sep-2024
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Glass syringe - the most worshiped artifact on The Nexus since the glass VaporGenie. The Nexus loves the glass.
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Communications-Security Analyst
Posts: 1280 Joined: 17-Aug-2014 Last visit: 05-Feb-2024 Location: Nirvana
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My 10ml glass syringes with 4" 12ga stainless steel dispenser gets used near daily.
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DMT-Nexus member
Posts: 557 Joined: 12-Jul-2012 Last visit: 01-Jan-2021
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Infrared spectrometer
Everything else I could make out of bubblegum and condom wrappers, or an eye dropper and an abnormally large rutabaga in the case of a sep funnel.
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analytical chemist
Posts: 7463 Joined: 21-May-2008 Last visit: 14-Jan-2025 Location: the lab
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I've seen DIY FTIR, DIY spectrophotometers, even DIY NMR. I've never seen DIY mass spec. "Nothing is true, everything is permitted." ~ hassan i sabbah "Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
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Crucify the ego, before it's far too late.
Posts: 45 Joined: 10-May-2015 Last visit: 01-Jul-2016
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Glass baster. I can improvise the rest. The baster is a must. Although I would prefer a separatory funnel. “Do not make the mistake of supposing that the little world you see around you - the Earth, which is a mere grain of dust in the Universe - is the Universe itself. There are millions upon millions of such worlds, and greater. And there are millions of millions of such Universes in existence within the Infinite Mind of THE ALL” ― Three Initiates, Kybalion
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