DMT-Nexus member
Posts: 111 Joined: 12-Oct-2014 Last visit: 21-Jul-2016
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(This post is regarding the limonene extraction of mescaline, but the answer to the question could be useful to other teks as well.)
I decided to finally tackle the job of evaporating the vinegar pulls that I've had sitting in mason jars for weeks. I am using Mew's suggested method of glass pie dishes in a modified Nesco food dehydrator. It works rather well actually, so thanks for that Mew!
Problem: The glass pie dishes have rounded edges that are making it difficult to collect 100% of the dried material. I can't get the edges using razor blades. I used a butter knife with a rounded edge, which gets some of it, but not all. I don't think I have anything that fits that curve well enough.
What is the best way to be 100% efficient in the evaporation stage? Is there a trick that you have learned? I searched for a while but couldn't find anyone talking about this yet.
Worst case scenario, I could just mop it up with a piece of tissue and eat it, having a little evaporation day celebration, and give up trying to collect it for cleaning with MEK.
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Posts: 7463 Joined: 21-May-2008 Last visit: 14-Jan-2025 Location: the lab
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in thermodynamic terms, nothing is ever 100% efficient. that being said, evaporation under reduced pressure saves a lot of time "Nothing is true, everything is permitted." ~ hassan i sabbah "Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
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![](/forum/resource.ashx?u=19032) DMT-Nexus member
Posts: 1311 Joined: 29-Feb-2012 Last visit: 18-Jul-2023
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You could add a small amount of vinegar to the dish to dissolve it all, then re-evap the vinegar on something with square edges.
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DMT-Nexus member
Posts: 111 Joined: 12-Oct-2014 Last visit: 21-Jul-2016
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benzyme wrote:in thermodynamic terms, nothing is ever 100% efficient.
that being said, evaporation under reduced pressure saves a lot of time What kind of vessel would you use to allow the easiest collection of dried material? Or is there a trick to getting it off of the glass, regardless of shape?
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DMT-Nexus member
Posts: 111 Joined: 12-Oct-2014 Last visit: 21-Jul-2016
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concombres wrote:You could add a small amount of vinegar to the dish to dissolve it all, then re-evap the vinegar on something with square edges.
Thanks Concombres, but I'm trying to avoid any redissolving/re-evaporation, since it causes loss of product. The output of the limonene tek is so low that even small losses are huge.
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