Hello again nexians
I have been making myself quite a bit of fumarate, via BLAB tek, but now that the last precip is dry i want to try freebasing it again
Last time i used one of the methods mentioned as part of the tek, where you make a paste with s carbonate then dry and pull with solvent, but that turned out to be quite a mess even tho it seemed to work fine
What i was thinking now was to adapt this method, dissolving the fumarates in water, then adding small amount of lye to freebase and pulling the water with xylene since i have a nice sep funnel anyway
Anyone know of losses doing it like this ? or problems?
All the methods for freebasing i found just seemed so unessecarily complicated or wasteful, like doing a cold precip in basified water ? pulling with naptha and freeze precip, instead of just using a good solvent and evap ?
am i missing something here? I heard freeze precip from solvent gives nicer looking crystals, but i like my jimjam and fat/plant/chem contaminants should already be negligible after limo-precip and then another freebasing+solvent pull right?
So yea, any advice ? Whats your favorite method for freebasing salts ?