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spawn9076
#1 Posted : 11/28/2014 9:29:24 AM

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So basically i used a modified Nomans Tek,

I used 200 grams of MHRB - roughly cut up with ordinary scissors and run through a blender really didn't cut it up at all very well chunks of MHRB went straight into a big glass container i have (4.7 liters).

I made a mix of sodium hydroxide (way more than need I know but assisted with size of glass container) 250 grams of sodium hydroxide and 3,750 ml de-ionised water. while it was still hot but the Sodium Hydroxide was fully dissolved I poured it into the container containing the MHRB.

I agitated this vigorously every ten minutes for 90 minutes.



I then added 600 ml of pure VM&P naptha. (this was experimental as I had heard less pulls was better)
I rolled the container around for 3 hours, I did not add heat I simply rolled it around for 3 minutes let it stand for 7 minutes and repeat. so in total it was 6 rolls of 3 minutes every hour that was 18 in total. I watched some anime whilst doing this to pass time.

I let it separate and decanted into my glass dish, 600ml was a hell of a lot for my tray and I popped it in the freezer for 12 hours.

results were far better than i had expected -
1,847 mg in one pull,
i poured off the naptha and allowed it my glass tray to rest upside down in the freezer for a further 3 hours,
then i pulled out this and allowed it to dry








I think this was a massive success and this will be my chosen future extraction method, I hope this benefits someone
 

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Pestile
#2 Posted : 11/28/2014 9:40:05 AM

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Beautiful! Laughing
 
spawn9076
#3 Posted : 11/28/2014 10:09:07 AM

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Pestile wrote:
Beautiful! Laughing


thanks Smile
 
concombres
#4 Posted : 11/28/2014 12:17:21 PM

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Drool
Keep pulling. If your bark is top quality thats only half your yeild Smile
I've come to expect 1g spice from every 50g so you may very well be able to pull something close to 4g from that soup.
 
spawn9076
#5 Posted : 11/28/2014 12:21:43 PM

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concombres wrote:
Drool
Keep pulling. If your bark is top quality thats only half your yeild Smile
I've come to expect 1g spice from every 50g so you may very well be able to pull something close to 4g from that soup.


I plan too gunna let my soup sit for a week or so I have plenty for now Smile
 
BenNice
#6 Posted : 11/28/2014 1:50:29 PM

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gorgeous! glad other people are starting to find good bark sources also, my last extraction gave me almost 3%! I think its good bark more than technique, at least with mine. cheers!!
 
Aweems
#7 Posted : 11/28/2014 10:26:13 PM

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Wow!🙈
That's a beautiful yield! Very happy

Nice work,
Happy travels ☺️👍
"You didn't ask for this, You didn't mean to.. It was all in the timing. This come to, this realization."
 
frobot
#8 Posted : 11/28/2014 11:13:18 PM

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Did you evap any of the 600ml of naphtha before freeze precipitating?
That seems like it would be a lot :O
 
spawn9076
#9 Posted : 11/29/2014 11:27:36 AM

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frobot wrote:
Did you evap any of the 600ml of naphtha before freeze precipitating?
That seems like it would be a lot :O


thats what i thought, i didn't evaporate anything at all and im using the solvent for the next pull. it worked really well, tbh it was an experiment because i left it in the freezer thinking maybe it would because there was too much naptha.

if it didnt i was going to evap some then freeze. turns out it worked great there must still be some DMT in the solvent that's why I'm re using it as well i think on the next pull i ill evap some first Smile
 
 
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