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Cleaning method for DMT extractions, not new, but worth a look. Options
 
CaptainFuture
#1 Posted : 11/3/2014 7:45:26 AM

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Dear Ones,
just want to share a method how to get out the DMT of Mimosa really fast with only ONE pull with close to zero Oxidation. And then to get out all white pure DMT with a new cleaning method. Honestly don't have the time to read much here myself, so if this is not new, forgive me.

First I extract the DMT with the following easy and fast AB extraction of 100grs of Mimosa bark shredded:
- I powderize the bark and use all material
- Slowly Cooking the bark 3 times, cooking down the combined extraction to roughly 200 to 250mls of liquid (3 times in each 2l of water with 20ml of 5% acetate acid)
- Cool down and while cooling add 20grs of lye
- Let sit for a few hours and pull with 350ml of room temp(not warm) Naphta
- Suck into a glass jar (not bowl, since no need to scrape it later), freeze precipe for 12hours.

With this method all DMT is pulled with one pull. Along with dust and dirt though. Cooking the extraction down that much ends in a dirty pull, but here comes the new cleaning method into action.

- I pour off the Naphta and use it later again, its now slightly yellowish, all red dirt is with the DMT sticking to the jar.
- I pour 300ml water with 15ml 5% acetate acid into the jar and shake. The DMT converts into the acetate salt and the dirt now colorize the water yellowish red.
- Basify with 20grs of lye
- Pull the DMT from this with 200ml of Naphta.
- Naphta comes out very clear and is freeze precipitated in a small glass BOWL.
- Scraped after 10hours this gives you 99% pure white fluffy DMT. Only a slight yellowish film collects at the bottom of the bowl from oxides(which are not cleaned with this method), if at all.

You can then surely recrystallize to have thicker crystals if wished.


Done this with 200grs of whole bark (not powdered bark) and got 2,5grs of pure whitish fluffy DMT.The very thin yellow layer seen in the pix was left behind, you can scrape of the DMT from above that. This yellowish DMT was another 100mgs.

Pix:

LOVE is all there is.
 

STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
Ambivalent
#2 Posted : 11/3/2014 8:20:55 AM

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like you said, this way of cleaning the spice has already been discussed here. its a mini a/b practically . nothing new. but thanx for the pics and your effort.
 
DreaMTripper
#3 Posted : 11/3/2014 8:22:52 AM

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A mini acid base/ back-salt isnt new but judging by the results your method is certainly an effective way to do an acid base.
 
Earthwalker
#4 Posted : 11/3/2014 8:33:20 AM

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Yeah nothing new and as documented here it's very effective and easy aswell !!Thumbs up

https://www.dmt-nexus.me...;t=58064&find=unread
 
CaptainFuture
#5 Posted : 11/3/2014 8:49:52 AM

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Thanks guys, I wonder that it's not more popular then, since I never came across it, till it came across me :-)

Anyway, saves a lot of cleaning with Naphta, so I'm thankful for that.
LOVE is all there is.
 
DreaMTripper
#6 Posted : 11/3/2014 9:07:54 AM

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Well like you said you dont have time to read much here Wink
How you did it though is neat and the results speak for themselves no hassle making multiple pulls not many teks ive read use that way, its just the reduction I found a pain when I tried something similar but having a small end solution is very convenient and easy to handle. Initially adding ethanol speeds that up.
 
endlessness
#7 Posted : 11/3/2014 9:12:33 AM

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What do you mean with all dmt goes in one pull? Did you do a second and third pulls to see if you yielded anything?

Also am I correct in understanding you are boiling 100g x3 using 4 liters of water for each boil? That seems like a LOT of water, did you try using less? Or do you mean that at the end you have 4 liters of water total after putting the 3 boils together?
 
CaptainFuture
#8 Posted : 11/3/2014 9:45:38 AM

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Sorry, you're truly right, I use 3times 2L :-) (I don't messure, but its a full pot, so maybe 2,5l, but not 4 :-))
Then cook down all extractions combined down to 250ml/300ml.

And 2nd pulls yielded not a single crystal,never. It's just crucial to use a lot of naphta for the one pull I do and to really mix it well, maybe even shake a bit.
LOVE is all there is.
 
Earthwalker
#9 Posted : 11/3/2014 10:06:49 AM

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So you use 300ml naps to you're boiled down soup of 300ml ?? Is you're soup alittle thick and does the equal part naps mix well !!
 
steppa
#10 Posted : 11/3/2014 10:26:44 AM

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Recently I thought by myself how nice it would be to have a one pull method.

I will give this a try. Thank you!
Everything is always okay in the end, if it's not, then it's not the end.
 
CaptainFuture
#11 Posted : 11/3/2014 11:03:15 AM

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It's great to only do one pull, and you can use the naphta still a few times, its not that dirty afterwards.

Its a thick (almost like Amazon Ayahuasca) liquid, yes. It's maybe only 250ml. (Look at the 900ml jar on the picture) I fill that jar up to 700ml I'd say, so 250ml extract and 350ml Naphta.
It will come out pretty dirty, since I don not use a coffee filter, only a tea colander. So dust is present which also goes in bits into the naphta.
But that all doesn't matter due to the easy clean with another AB afterwards.

It is a fast, easy and effective way, that's what I'm saying, having extracted a lot the past years.
And I always used that long taking naphta cleaning method.

Be sure to use room temp Naphta, that helps to avoid oxidation.

PLEASE share your experiences with it here.
LOVE is all there is.
 
tydel24
#12 Posted : 10/10/2015 12:37:08 PM

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The pulls may look clear as a window... Buy let that sit for a few hours.. Then observe the goo on the bottom.. That goo Is what taints the spice..its very psychoactive however. And it is my.preference.. Evap at a steady pace.. But not enough to where you see crystals drop.. Pour your now enriched sllvent away from the goo by changing your dish.. Careful not to pour any of the migrating goo..seal the dish.. Freeze... Let excess solvent evap away from the goo..then scrape that jungle.
I.store it all in a shot glass and keep it wrapped and open at top for dry..refrigerate.. After.
 
 
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