Hi Clockwork Maggot! I am indeed a dude FYI, and the calls to Major Tom will not cease until he decides to answer me!
I used a tek I found online (http://www.shroomery.org/forums/showflat.php/Number/11940270) that involved boiling in lye and then extraction with naphtha. Pretty similar to a lot of teks I've read about. My problem was that in a wide steel pot I wasn't able to get the naphtha to rise and separate it from the black nasty lye goop. So I added way too much naphtha thinking that If I added enough I would be able to form a layer thick enough to separate. Still no success.
I was soooo close to giving up on the whole process and dumping out my black pot of poison. Then I did a little more reading (I believe it was Orion's Tek from this site) and transferred the whole mixture into a large glass bottle with a neck and voila! The naphtha separated from the lye solution enough for me to extract it without problem. Then my problem was that I had way too much naphtha for the amount of MHRB I used (50g). So I had to do three freezer precipitations, and evaporate some of the naphtha under a fan.
Long story short, the first precipitation yielded beautiful, big, fluffy crystals - mostly white and a couple yellow, but not a lot in terms of weight. The second precipitation was a little less productive, but then I evaporated a good deal of the naphtha and the third precipitation yielded small crystals, but by far the most spice. I'm doing a fourth and final precipitation tonight and I'm hoping the yield is like today's. I sampled the finished product last night and it's grade A stuff in my book. I think by the end of the whole process I'll end up with a 1.5% to 2% yield, which makes me a happy camper.
I'm very happy that I can rely on myself for this from now on, and now I just need to find a good supplier of MHRB. I used Avalon Magic Plants for my first test order, but now they're out of stock.
~Peace, Love, and Discretion~