We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Extracting San Pedro with basic methanol? Options
 
chiggels
#1 Posted : 7/19/2014 10:10:47 AM

DMT-Nexus member


Posts: 56
Joined: 05-Apr-2014
Last visit: 13-Aug-2014
Brain's getting some more cacti next week and he is wondering if he can extract it using a methanol/NaOH solution. He has heard, from quite a few people, that prolonged exposure to NaOH degrades mescaline. So is that going to be a problem?
All of my posts are Pinky and The Brain fan fiction.
 

STS is a community for people interested in growing, preserving and researching botanical species, particularly those with remarkable therapeutic and/or psychoactive properties.
 
Nathanial.Dread
#2 Posted : 7/19/2014 2:23:01 PM

DMT-Nexus member


Posts: 2151
Joined: 23-Nov-2012
Last visit: 07-Mar-2017
Both of these from The Nexus Wiki:

69Ron's D-Limonene Extraction
https://wiki.dmt-nexus.m...ene_Mescaline_Extraction

Kash' A/B Extraction
https://wiki.dmt-nexus.m...A/B_Mescaline_Extraction

Between the two of them, those should take care of all your mescaline extraction needs.

Blessings
~ND
"There are many paths up the same mountain."

 
Ufostrahlen
#3 Posted : 7/19/2014 4:29:09 PM

xͭ͆͝͏̮͔̜t̟̬̦̣̟͉͈̞̝ͣͫ͞,̡̼̭̘̙̜ͧ̆̀̔ͮ́ͯͯt̢̘̬͓͕̬́ͪ̽́s̢̜̠̬̘͖̠͕ͫ͗̾͋͒̃͛̚͞ͅ


Posts: 1716
Joined: 23-Apr-2012
Last visit: 23-Jan-2017
chiggels wrote:
Brain's getting some more cacti next week and he is wondering if he can extract it using a methanol/NaOH solution. He has heard, from quite a few people, that prolonged exposure to NaOH degrades mescaline. So is that going to be a problem?


In theory, this could work. Mesc base is soluble in Methanol.

http://www.swgdrug.org/Monographs/PEYOTE.pdf

Best way is to try and find out.

Also check out: https://www.dmt-nexus.me...&m=245189#post245189
Internet Security: PsilocybeChild's Internet Security Walk-Through(1)(2)(3)(4)(5)(6)(7)(8)
Search the Nexus with disconnect.me (anonymous Google search) by adding "site:dmt-nexus.me" (w/o the ") to your search.
 
dg
#4 Posted : 7/19/2014 9:39:44 PM
DMT-Nexus member

Cacti expert

Posts: 1175
Joined: 10-Jun-2010
Last visit: 27-Dec-2024
chiggels wrote:
. He has heard, from quite a few people, that prolonged exposure to NaOH degrades mescaline.


quite a few people would be wrong

wont be a problem, but what are you going to do to get your mesc from the basic alcohol?

 
chiggels
#5 Posted : 7/21/2014 1:40:45 AM

DMT-Nexus member


Posts: 56
Joined: 05-Apr-2014
Last visit: 13-Aug-2014
Distill off most of the methanol.
Acidify with HCl.
Wash with acetone.
Dry.
All of my posts are Pinky and The Brain fan fiction.
 
dg
#6 Posted : 7/21/2014 2:30:12 AM
DMT-Nexus member

Cacti expert

Posts: 1175
Joined: 10-Jun-2010
Last visit: 27-Dec-2024
i think you'll end up with a salty product, lye plus hcl....

 
chiggels
#7 Posted : 7/21/2014 3:53:56 AM

DMT-Nexus member


Posts: 56
Joined: 05-Apr-2014
Last visit: 13-Aug-2014
What if he acidifies with acetic acid(produces sodium acetate), dries the neutralised stuff, then washes it with cold MEK to remove non mescaline alkaloids? Good way to get mescaline acetate?
All of my posts are Pinky and The Brain fan fiction.
 
dg
#8 Posted : 7/22/2014 2:42:16 AM
DMT-Nexus member

Cacti expert

Posts: 1175
Joined: 10-Jun-2010
Last visit: 27-Dec-2024
mek wash probably wont be terribly effective, i'd distill off the methanol, make sure its basic to 13 or so and pull with nps.
nice way to reduce nps use in an extraction imo, but have never tried it

then carefully salt it out in what ever form you want
careful titration during salting yields a much nicer produt
 
 
Users browsing this forum
Guest

DMT-Nexus theme created by The Traveler
This page was generated in 0.035 seconds.