Hi guys, I'm reading the recrystallization tek here https://www.dmt-nexus.me...aspx?g=posts&m=10545 and I wanted to be clear on steps 16-19 before proceeding. here are the instructions


16. Remove shotglass from waterbath. Notice the separation of oils.
17. Use eye dropper to suck up yellow oils and squirt into second shotglass.
Note: In that new shotglass oil will sink and any DMT solvent you grabbed will float.
18. Tilt the second shotglass and suck back out any remaining clean DMT solvent and add back to original shotglass.
Note: As an alternative the clean solvent can be poured back into the original shotglass as the oil will stick to the bottom.
19. Take first shotglass with DMT solvent and pour into a third clean shotglass. The little bit of oil remaining will stick to the bottom of the glass.


So in step 17 you are supposed to put the eye dropper all the way to the bottom of the first shot glass and suck up the nasty goo on the bottom, then squirt that into a second empty shot glass.

after this you tilt the second shot glass and attempt to pull any clean solvent and then add that to the first shot glass. Should I wait any period of time before doing this for it to settle, or do I do it right away?


any other tips on recrystallization would be appreciated, thanks

I did not think it took 22 steps to re-x. But okay, if it works for you do it.

It should happen right away. If you are waiting longer than 10 minutes for anything to appear on top of the second shot glass and nothing is showing up, then its because what you sucked up didn't contain any extra solvent.

As 18 hints at, you can easily just pour off the extra solvent in the second shot glass. No need to suck anything back up. If you cant pour anything off then i would say you're good to go.

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