Also, an easy way to get pure mhrb fumarate alkaloids, is to do a standard acid base acid cook/reduction, evap that to a resin. Mix it 2:1 lime (caoh:mhrb), add enough water to make a watery paste. Dry it overnight, but keep it out of light/high temps.

Take your dried basified resin, pull 3x with DRY acetone, decanting or filtering out any sediment, and add fumaric acid saturated acetone to the combined 3 acetone pulls you now have. You'll instantly notice clouding, then precipitation of fairly pure dmt fumarate crystals.

Once it stops clouding let it sit in a sealed container for a few hours, then add more fasa (fumaric acid saturated acetone) until it no longer clouds. Waiting a few hours between each addition of the fasa. You can't add too much fasa, since any fumaric acid will be soluble in the acetone you pulled with, but its best to be as efficient and frugal with your extraction supply's, so try and conserve your fasa/acetone. No need for waste here Thumbs up

You can use acetone to pull spice but it has to be dry because acetone is miscible with water so you can't separate them.
And if there is water in your acetone you can't precitate salts as they are soluble in this water.




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You can easily turn hardware store acetone into anhydrous acetone with the simple process I've outlined below. To do this, you'll need to go to Home Depot or Lowes and get the following items: a 1 liter can of acetone and a bag of epsom salts.

Heat some epsom salts on an aluminum foil covered baking sheet in the oven for 2 hours at 400 degrees F. After 2 hours of heating, the epsom salts have now been turned into anhydrous magnesium sulphate. Crazy huh?

Take 10-20 grams of your greyish ash looking anhydrous magnesium sulphate and pour it directly into your can of hardware store acetone. Shake the can vigorously for a few minutes to circulate the magnesium sulphate and then let it settle for 24 hours. The magnesium sulphate will absorb all of the water and/or alcohol from the hardware store acetone and sink it to the bottom of the can where it shall remain forever.

Therefore from now on, never pour from the can, instead use a glass eye dropper or glass pipette (glass straw) to reach down inside of the can to extract however much anhydrous acetone you'll be requiring. Always stay away from the bottom of the can. Once the can get's about half way down, discard and repeat the process with a fresh can of acetone. Always use glass hardware when using acetone. Acetone will melt plastic.

Im no expert but the theory in the OP seems legit no reason I can see that it wouldnt work its a tweaking of the BLAB tek but its unlikely to be very pure as there has been no separation from the polar impurities and then when using acetone to paste and pull will pull all the impurities with it, some will stay in the acetone after doing the FASA but some will no doubt precipitate with the full spec fumarates and may stop some of the fumarates precipitating in the first place.

Infundibulums tek looks really neat but he said himself the effectiveness may depend on using lab grade chemicals. It also renders the acetone unuseable after meaning a great deal of waste is generated.

Can you get limonene? Must be able to sunflower oil, for sunflower/vege oil you could do an a/b and salt out using FASW evaporate the water off then wash with anhydrous acetone to remove excess fumaric acid.
Or if you can get ethanol you could follow endlessnesses
tek here https://www.dmt-nexus.me...aspx?g=posts&t=30501
then once youve got the extract after the cleanup steps you could dissolve it in acetone and FASA it.

it mention Heating some epsom salts on an aluminum foil in an oven to convert to anhydrous magnesium sulphate. If I only get magnesium sulphate and mix it in acetone, will it create anhydrous acetone? if not how do I make anhydrous magnesium sulphate, from normal magnesium sulphate?

And also, by the way, I can get 99.7% acetone, that's what my supplier says. Is it enough "anhydrous" already?

Thank you.

One more thing though, with the magnesium sulfate, can I do the heating like everything described in the method but with stove fire(not microwave oven). And I may not know the temp of fire though. Can I over heat it and end up turning it into something else other than anhydrous magnesium sulfate?

Thank you.

Can I over heat it and end up turning it into something else other than anhydrous magnesium sulfate?

Rendering Crystalline DMT Fumarate

Dissolve about 7mg fumaric acid per mL of fresh anhydrous acetone to prepare a FASA solution, allotting adequate time and stirring for complete saturation, and allowing any excess to settle to the bottom.
It is recommended that the solution be prepared in slight excess of fumaric acid rather than an excess of acetone for the procedure to be most effective.

From the wiki (here)