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over-reduction of vinegar boils? salvageable? Options
 
Leon Trout
#1 Posted : 4/13/2014 5:03:00 PM

when in doubt, twirl


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so yesterday i started an extraction on 1kg of ACRB... used thicklight's tek, it's always worked before...

while reducing my vinegar boils, i sort of napped off & reduced them more than i wanted to... when i woke, i had a very thick liquid left in my pot... i let it sit overnight, & now i have a thick sludge... not very liquidy at all... my first instinct is to boil the sludge in some fresh vinegar/h20... is this a viable path to saving this, or am i just S.O.L. on this one?..
spinning a set the stars through which the tattered tales of axis roll about the waxen wind of never set to motion in the unbecoming round about the reason hardly matters nor the wise through which the stars were set in spin...

"Chemistry is applied theology." Augustus Owsley Stanley III
 

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endlessness
#2 Posted : 4/13/2014 5:41:53 PM

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Only one way to find out Very happy

I bet you`re fine though.. Just add a bit of water and mix it, no need to boil more.

Good luck!
 
Leon Trout
#3 Posted : 4/13/2014 5:55:14 PM

when in doubt, twirl


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thanks... that's what i'm hoping... it was a real heart-sinking feeling to look in my pot this morning only to find a mud that wouldn't even pour... made that eternity spent boiling yesterday feel like 2 of 'em... gonna keep my fingers crossed, i'll post results when i have some...
spinning a set the stars through which the tattered tales of axis roll about the waxen wind of never set to motion in the unbecoming round about the reason hardly matters nor the wise through which the stars were set in spin...

"Chemistry is applied theology." Augustus Owsley Stanley III
 
cubeananda
#4 Posted : 4/13/2014 9:10:46 PM

jai


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Yeah as long as it didn't burn it should be fine. Freebase it and if you want to go oral route use like orange juice or a more friendly acid.
 
Leon Trout
#5 Posted : 4/13/2014 10:15:40 PM

when in doubt, twirl


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pretty sure it didn't burn, when i woke up there was still 2+ liters of liquid, albeit a vigorously boiling liquid...

i added the 2000ml of additional water/vinegar & put it on the stove to steep for 15 minutes or so... chilled in the fridge & filtered 2x... recovered 2100 ml, split it into 3 jars & salted... gonna add base shortly & pull at least one jar later tonight... i've got a decent feeling all will be okay...
spinning a set the stars through which the tattered tales of axis roll about the waxen wind of never set to motion in the unbecoming round about the reason hardly matters nor the wise through which the stars were set in spin...

"Chemistry is applied theology." Augustus Owsley Stanley III
 
DreaMTripper
#6 Posted : 5/6/2014 1:26:07 PM

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2l is plenty but you shouldnt leave it unattended while you sleep.
 
Earthwalker
#7 Posted : 5/6/2014 3:02:55 PM

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DreaMTripper wrote:
2l is plenty but you shouldnt leave it unattended while you sleep.


So you say aslong as you're next to the pot it's ok to have a nap !! Big grin
 
DreaMTripper
#8 Posted : 5/7/2014 5:01:36 AM

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Correct! Make sure you sleep with your head on the lid so if it boils over you'll know!
Or dangle your nackers in it so you know when its too hot just like running a bath!
 
Earthwalker
#9 Posted : 5/7/2014 8:06:12 AM

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DreaMTripper wrote:
Correct! Make sure you sleep with your head on the lid so if it boils over you'll know!
Or dangle your nackers in it so you know when its too hot just like running a bath!

Laughing
 
 
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