I performed a standard A/B with phosphoric acid and lye on MHRB, first pull was freeze precipitated with naphtha but for the second pull I wanted to try FASA, I used xylene for the pull and salted it with my FASA solution of 100ml anhydrous Acetone + 0.7g fumaric acid that completely dissolved.
Upon adding the FASA solution dropwise to the xylene it became very cloudy and I left my container covered with a plastic bag and a rubber band to avoid evaporation of the acetone for 48 hours.
Crystals formed in the container and when the solution was completely clear I removed the Xylene/Acetone with a pippete, the results are pictured below. My concern is that the fumaric acid was kicked out of solution and I have a mixture of fumaric acid + DMT fumarate because I'm not sure if the crystalization is normal when salting out with FASA: