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Freeze-precip carrying contaminants from solvent Options
 
mrdruid0
#1 Posted : 2/1/2014 8:08:49 PM
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Hey there everyone

One would wonder if possible contaminants in a solvent will be transferred to the product in very small amounts of solvent left in the crystal matrix after pouring off?

Or does freeze-precipping and pouring off successfully remove all worry-worthy contaminants?
 

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wearepeople
#2 Posted : 2/1/2014 8:20:52 PM

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A thorough read of §10 of the health and safety (see the link below the banner at the top of the page?) would be good for you.

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mrdruid0
#3 Posted : 2/1/2014 8:43:17 PM
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wearepeople wrote:
A thorough read of §10 of the health and safety (see the link below the banner at the top of the page?) would be good for you.

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Thanks!

I've read it thoroughly, multiple times.

Even though a solvent evaps clean and is as pure as one can guarantee, there is always the possibility of trace contamination and thus the possibility of anxiety thereof. I am wondering if freeze-precipitation is more likely to protect me from possible contamination then evaporation.

Any constructive replies?
 
hopefull
#4 Posted : 2/1/2014 10:58:20 PM

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I think as long as you use actual naphtha there should be no worries. I think if you use some junk lighter fluid as a solvent it can leave residue
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Auroas
#5 Posted : 2/5/2014 7:31:26 PM

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expandaneum
#6 Posted : 2/5/2014 9:36:57 PM

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read some more as this question is covered extensively

I would start here
https://www.dmt-nexus.me...aspx?g=posts&t=11715

take care
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