We've Moved! Visit our NEW FORUM to join the latest discussions. This is an archive of our previous conversations...

You can find the login page for the old forum here.
CHATPRIVACYDONATELOGINREGISTER
DMT-Nexus
FAQWIKIHEALTH & SAFETYARTATTITUDEACTIVE TOPICS
Freeze Precip Options
 
hedcase
#1 Posted : 4/22/2009 12:36:18 AM

DMT-Nexus member


Posts: 126
Joined: 21-Apr-2009
Last visit: 18-Jun-2010
Location: The Great White North
I'm doing preliminary research on extraction, and have a question.Once I separate saturated solvent,can I put it directly into a mason jar into the freezer?Should the solution be evaporated somewhat before?If so can I do this in the same mason jar?Any help is much appreciated...
On my back and tumbling
Down that hole and back again
Rising up
And wiping the webs and the dew from my withered eye.
 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
everythingsflashin
#2 Posted : 4/22/2009 1:38:04 AM
DMT-Nexus member


Posts: 65
Joined: 03-Mar-2009
Last visit: 19-Dec-2009
Location: Nirvanaland
SWIM did 4 1000ml pulls for 1kg of mimosa and put them all directly in the freezer. worked just fine. no evaporating. but evaporating it some wouldnt hurt either.
Your body is just a vehicle, transporting your soul.
 
hedcase
#3 Posted : 4/22/2009 1:49:03 AM

DMT-Nexus member


Posts: 126
Joined: 21-Apr-2009
Last visit: 18-Jun-2010
Location: The Great White North
everythingsflashin wrote:
SWIM did 4 1000ml pulls for 1kg of mimosa and put them all directly in the freezer. worked just fine. no evaporating. but evaporating it some wouldnt hurt either.
how long did it take SWIM to obtain xtals?Did SWIM pour off solvent and dry in the same jar?
On my back and tumbling
Down that hole and back again
Rising up
And wiping the webs and the dew from my withered eye.
 
Fatcat
#4 Posted : 4/22/2009 5:05:22 PM

DMT-Nexus member


Posts: 198
Joined: 04-Mar-2009
Last visit: 27-Sep-2015
Location: That Great Gig in the Sky
I recommend warming the naptha first, one so it will dissolve more crystals, and two it will evaporate faster. After the solution is saturated I put it on my portable burner to evap. I normally try to get around 25% evaporation. Then I put it in the freezer for AT LEAST 24 hours (I have found that if you are impatient you can pour out the milky solvent into another container and scrape the barley formed crystals for little pre harvest, as i like to call it), or until solvent is clear, and then some.
By allowing this message to pass through your cornea, into your retina, you accept it as is and agree to my disclaimer regarding my posts that they are a complete falsification by doing so freeing me of all liability, direct, indirect, consequential or incidental that may arise from the instillation of this post in your memory bank.
 
hedcase
#5 Posted : 4/22/2009 10:28:18 PM

DMT-Nexus member


Posts: 126
Joined: 21-Apr-2009
Last visit: 18-Jun-2010
Location: The Great White North
Fatcat wrote:
I recommend warming the naptha first, one so it will dissolve more crystals, and two it will evaporate faster. After the solution is saturated I put it on my portable burner to evap. I normally try to get around 25% evaporation. Then I put it in the freezer for AT LEAST 24 hours (I have found that if you are impatient you can pour out the milky solvent into another container and scrape the barley formed crystals for little pre harvest, as i like to call it), or until solvent is clear, and then some.

What is the safest way to warm naphta?
On my back and tumbling
Down that hole and back again
Rising up
And wiping the webs and the dew from my withered eye.
 
Nzym
#6 Posted : 4/22/2009 10:38:22 PM

DMT-Nexus member


Posts: 55
Joined: 26-Mar-2009
Last visit: 19-Mar-2010
Location: Just above the stratosphere.
Make a warm water bath. Take a pan and add water, then bring it to a boil. Then partially submerge a jar with the naptha into the pan in such a way that doesn't directly contact the heat source (if your glass isn't Pyrex or lab quality, it will likely shatter if left on direct heat); SWIM uses a steel strainer with a lip that catches onto edge of the pan to hold the jar in the water like on this thread. Let it sit there for a while (SWIM does 10-20 minutes) under constant attention. And that's it.
 
endlessness
#7 Posted : 4/22/2009 10:41:02 PM

DMT-Nexus member

Moderator

Posts: 14191
Joined: 19-Feb-2008
Last visit: 30-Jan-2025
Location: Jungle
Pre evaporating to maybe a quarter of original amount will make more crystals crash out. But if one wants to save on solvent, can try to make a bigger amounts of small warm pulls, straight in the freezer, collect whatever comes out and reuse the naphtha for more pulls.

for warming naphtha before its in the solution, heat some water in a pot to near boil, then turn off the fire. Have the solvent in another opened small glass container that is easy to pour out off, and submerge the bottom part of the glass with the solvent in the warm water, and let it stay for a few minutes. Take off the glass bottom from warm water and pour solvent into the mimosa mix. Careful because many times the solvent drips down the side of the glass.

I would not suggest warming naphtha for evaporation, you risk evaporating some of the dmt. Better use a fan instead (with a thin cloth over to prevent dust)
 
everythingsflashin
#8 Posted : 4/22/2009 10:43:21 PM
DMT-Nexus member


Posts: 65
Joined: 03-Mar-2009
Last visit: 19-Dec-2009
Location: Nirvanaland
SWIMs crystals started to form after about 5 hours, but didnt finish till about 24 hours.
Your body is just a vehicle, transporting your soul.
 
hedcase
#9 Posted : 4/22/2009 11:53:33 PM

DMT-Nexus member


Posts: 126
Joined: 21-Apr-2009
Last visit: 18-Jun-2010
Location: The Great White North
endlessness wrote:
Pre evaporating to maybe a quarter of original amount will make more crystals crash out. But if one wants to save on solvent, can try to make a bigger amounts of small warm pulls, straight in the freezer, collect whatever comes out and reuse the naphtha for more pulls.

for warming naphtha before its in the solution, heat some water in a pot to near boil, then turn off the fire. Have the solvent in another opened small glass container that is easy to pour out off, and submerge the bottom part of the glass with the solvent in the warm water, and let it stay for a few minutes. Take off the glass bottom from warm water and pour solvent into the mimosa mix. Careful because many times the solvent drips down the side of the glass.

I would not suggest warming naphtha for evaporation, you risk evaporating some of the dmt. Better use a fan instead (with a thin cloth over to prevent dust)

Awesome!!!I'm about to order my first lb of bark..
On my back and tumbling
Down that hole and back again
Rising up
And wiping the webs and the dew from my withered eye.
 
 
Users browsing this forum
Guest (2)

DMT-Nexus theme created by The Traveler
This page was generated in 0.020 seconds.