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N-Hexane Options
 
stoj
#1 Posted : 7/6/2013 9:11:41 PM
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HI TO ALLSmile
i just joined so i first would like to say hello to all.

im about to order my supplies for my dmt extract however i dont want to use zipo lighter fluid or similar. i want to use N-Hexane is this the best chemical to use? i was thinking to use acetone after to clean and residue after would this be best way?
 

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stoj
#2 Posted : 7/8/2013 1:06:14 PM
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can any one help me please? i am able to get hold of pretty much any chemical but need some of your help the best and safest way to do this. i can not seem to find naphtha in the uk labeled as that any way. i do have naphtha (petroleum)
hydrotreated, heavy (EC 265-150-3) i have tested this and its evaporation is very slow and burns with black smoke not good? However i have heard that the heavy is better for pulling out the DMT? any advice will be much appreciated?

thanks STOJ
 
endlessness
#3 Posted : 7/8/2013 1:29:52 PM

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Acetone for clean up, how? Acetone dissolves dmt and all the impurities, unless you use FASA method. Read the FAQ please.


i would not advice using heavy naphtha, it's a pain in the ass to work with it, and can taint your final product with traces.

Hexane should work perfectly fine, if you can find it.
 
Jees
#4 Posted : 7/8/2013 5:12:32 PM

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If you're UK, this thread might help:
What actually is the cleanest solvent to use for exaction in UK

Your naphta EC 265-150-3 is a white spirit C11 - C12:
http://www.macduck.co.za/msds/dual_action_2.pdf
that's as heavy as the Australian Ayers Rock Crying or very sad
 
benzyme
#5 Posted : 7/8/2013 5:20:27 PM

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if you can get the dmt free base to dissolve in warm hexane, freeze precipitate it.
hexane is one of the best solvents for recrystallization.
I prefer it over heptane because of its lower b.p.
"Nothing is true, everything is permitted." ~ hassan i sabbah
"Experiments are the only means of attaining knowledge at our disposal. The rest is poetry, imagination." -Max Planck
 
stoj
#6 Posted : 7/9/2013 2:12:28 AM
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hi thanks all for the replies very much appreciated.
i have now ordered hexane which should be here next few days i will keep your all posted with some pictures hopefully all goes well.
i must say i am little worried doing it for my first time however i have tried to prepare my self for many weeks.
would it be ok to do it on my own for first time? smoking it this is, or to have a sitter?

and thanks again for the repliesThumbs up
stoj attached the following image(s):
.jpg,.JPG (2,078kb) downloaded 114 time(s).
 
stoj
#7 Posted : 8/4/2013 1:11:55 PM
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hi, all thought i would update, this is what a managed to pull from 2 extractions.
using hexane

tried 30mg last night using a plastic bong with foil with dmt on top of some ashes, didnt seem to harsh,

took 2 hits and held it in,
what happend?
ok i had real heaveness on my hole body and funny vibrating feelin, no real blast off but i had some really weird pictures in the mirror that was in front of me the mirror started to bend and vibrate then it was like lots of images of faces? i think they were there was so many faces.
i was relaxed but when i shut my eyes not much happend?

?
any thoughts does my spice look ok ?

i weighed on some scales 0.030g but not sure if i took enough?

how to eyeball enough dmt?
 
stoj
#8 Posted : 8/4/2013 3:12:50 PM
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benzyme wrote:
if you can get the dmt free base to dissolve in warm hexane, freeze precipitate it.
hexane is one of the best solvents for recrystallization.
I prefer it over heptane because of its lower b.p.



thanks for the reply, which is best chemical for extracting dmt? uk does not sell vmp naptha

i do have colmens fuel uk version ?

is hexane best for extracting you just re-x ?

my picture below was hexane to extract dmt and freeze but not much white crystals?
 
 
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