 DMT-Nexus member
Posts: 45 Joined: 07-May-2013 Last visit: 20-Mar-2014
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Hi Nexians!
Anyone have an easy chali tek? Lextek has been suggested elsewhere. Also, once the extraction is done, how does one seperate the 5-meo and the N-N-DMT?
Thanks!
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 Dreamoar
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Posts: 4711 Joined: 10-Sep-2009 Last visit: 24-Feb-2025 Location: Rocky mountain high
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 Kalt und Heiß, Schwarz und Rot, Kürper und Geist, Liebe und Chaos
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Posts: 4661 Joined: 02-Jun-2008 Last visit: 30-Apr-2022
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STB also works fine with chaliponga. Need to calculate between salts and freebases? Click here! Need to calculate freebase or salt percentage at a given pH? Click here!
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 DMT-Nexus member
Posts: 45 Joined: 07-May-2013 Last visit: 20-Mar-2014
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STB with the leaf? I've tried that and it's didn't work.
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 Kalt und Heiß, Schwarz und Rot, Kürper und Geist, Liebe und Chaos
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Posts: 4661 Joined: 02-Jun-2008 Last visit: 30-Apr-2022
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Fungaai wrote:STB with the leaf? I've tried that and it's didn't work. Weird- do you mind describing your method? What exactly did not work and how did you assess failure? I've done STB in chaliponga in a few times in the past, with success. I've pulled with naphtha as well as xylene. Need to calculate between salts and freebases? Click here! Need to calculate freebase or salt percentage at a given pH? Click here!
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 DMT-Nexus member
Posts: 45 Joined: 07-May-2013 Last visit: 20-Mar-2014
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I used xylene. Don't know if I have the PH right though. I used 37.5g of NAOH in 500ml water. Don't know if that's too much.
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 DMT-Nexus member
Posts: 45 Joined: 07-May-2013 Last visit: 20-Mar-2014
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If the yellowish green goo end product indicates success. How does one clean it up? I hot naphtha, but all of it dissolves.
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 Kalt und Heiß, Schwarz und Rot, Kürper und Geist, Liebe und Chaos
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Posts: 4661 Joined: 02-Jun-2008 Last visit: 30-Apr-2022
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You've got to be more descriptive, also see this tread for more instructions. As you realise, it is hard to get helpful feedback if you do not describe your process thoroughly. How much material did you use, dissolved in how much water, what did you do after you collected your xylene pull etc etc.... Need to calculate between salts and freebases? Click here! Need to calculate freebase or salt percentage at a given pH? Click here!
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 DMT-Nexus member
Posts: 45 Joined: 07-May-2013 Last visit: 20-Mar-2014
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Okeydokey...
500ml water with 37.5g of NAOH dissolved. Shaken and stood for an hour. Added 50ml of xylene and shaken intermittently for 12 hours Added 50ml of xylene and shaken intermittently for 12 hours wait for seperation Siphon of xylene Repeat above steps Combine xylene and evap. The end result is a yellowish-green syrup. Then a naphtha recrystallization was attempted assuming the DMT would be taken into the solvent and everything else would stay behind. All the syrup was dissolved in the solvent instead.
Any ideas?
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 DMT-Nexus member
Posts: 1369 Joined: 22-Jan-2010 Last visit: 07-Mar-2014
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standard a/b works fine. boil leaves, reduce if you want. base it, solvent it, fasa it, then convert to freebase with sodium carb, or just leave it as fumarate.
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