Mostly Ignored
Posts: 560 Joined: 25-Feb-2013 Last visit: 07-Mar-2014
|
Gotcha.. I was here hoping to hear about increased yields hehehe  I got about 600ml of Ronsonol left then I may give Swan a go  As always, Thanks Cyb 
|
|
|
|
|
DMT-Nexus member
 
Posts: 3574 Joined: 18-Apr-2012 Last visit: 05-Feb-2024
|
ZenSpice wrote:Gotcha.. I was here hoping to hear about increased yields hehehe Moar Salt  Please do not PM tek related questions Reserve the right to change your mind at any given moment.
|
|
|
DMT-Nexus member
Posts: 2807 Joined: 19-May-2009 Last visit: 16-Mar-2024
|
If yield is what your after, check out the BLAB tek, orange oil aka limonene is used. their are a few extra steps inolved in the extraction process, but well worth it, and bonus is that you will have fumarate for oral use. ahhh the fresh citrus smell, yummy.
|
|
|
Michael
Posts: 175 Joined: 01-Nov-2010 Last visit: 10-Dec-2024 Location: UK
|
How about Heptane? according to some on here it is just as good as Hexane. i have just bought some and used it in cybs tek for the first couple of pulls. nice solid crystals. Here is the link, £6 for 2 litres delivered! evaps totally clean and is pure Heptane. and when the world stops
you will find me there
waiting to embrace you
|
|
|
DMT-Nexus member
Posts: 3574 Joined: 18-Apr-2012 Last visit: 05-Feb-2024
|
Yes Orion reports Heptane to be very good (Tetrosyl panel wipe). I plan to use this on the next run. Please do not PM tek related questions Reserve the right to change your mind at any given moment.
|
|
|
Mr Invisible
Posts: 43 Joined: 12-May-2013 Last visit: 30-May-2013 Location: Orions Belt
|
I have tried evaping bartoline but that leaves residue...and zippo ... its fairly clean but there is still residue.... Still waiting for the tetrosyl panel wipe to arrive, I will post results... not that anyones bothered about what i say, apparently i should be banned from the site. and that iiiii'mmm semi bloody illiterate.... Its an absolute outrage.. A Bloody Embarresment, i think ive posted some bloody good stuff lol "It Never Got Weird Enough For Me"..... But I Have A Feeling I'm About To Reach A Whole New Fucking Level!!!!
|
|
|
Michael
Posts: 175 Joined: 01-Nov-2010 Last visit: 10-Dec-2024 Location: UK
|
cyb wrote:Yes Orion reports Heptane to be very good (Tetrosyl panel wipe). Tetrosyl panel wipe is Hexane Cyb. The link in my last post is for Heptane.  and when the world stops
you will find me there
waiting to embrace you
|
|
|
DMT-Nexus member
Posts: 4031 Joined: 28-Jun-2012 Last visit: 05-Mar-2024
|
Thank you very much for valuable information in this thread <3
|
|
|
DMT-Nexus member
Posts: 3574 Joined: 18-Apr-2012 Last visit: 05-Feb-2024
|
Kerberos wrote:
Tetrosyl panel wipe is Hexane Cyb.
Thanks Kerboros...I stand corrected A momentary lapse.Please do not PM tek related questions Reserve the right to change your mind at any given moment.
|
|
|
Mostly Ignored
Posts: 560 Joined: 25-Feb-2013 Last visit: 07-Mar-2014
|
Triple filtered kudos for all the intel
|
|
|
DMT-Nexus member
Posts: 14 Joined: 25-Apr-2012 Last visit: 13-Apr-2016 Location: Canada
|
Kerberos wrote:How about Heptane? according to some on here it is just as good as Hexane. i have just bought some and used it in cybs tek for the first couple of pulls. nice solid crystals. Here is the link, £6 for 2 litres delivered! evaps totally clean and is pure Heptane. So, you can totally substitute Naphtha in Cyb's for that pure Heptane? I was thinking I may have to do this but I am really too unclear on how to go about it, would you mind clarifying on how you managed it?
|
|
|
Michael
Posts: 175 Joined: 01-Nov-2010 Last visit: 10-Dec-2024 Location: UK
|
mrdruid0 wrote:So, you can totally substitute Naphtha in Cyb's for that pure Heptane?
I was thinking I may have to do this but I am really too unclear on how to go about it, would you mind clarifying on how you managed it? I warmed the Heptane, 50ml, and added it instead of the naphtha. I did this twice just as an experiment. The Heptane was then put in a pyrex dish and allowed to evaporate overnight. I scraped together the resulting crystals which were in the main very clean with a slightly yellow residue on the base of the dish. From two pulls i got 612mg using Cybs tek with 50g of MHRB. (I did another 4 pulls with naphtha and these are in the freezer.) So just substitute the word Heptane for the word Naphtha in the tek and your good to go. I dont know if you can freeze precip Heptane hopefully someone will chime in with this info. I will be doing Cybs tek again but this time i am going to use isoHexane and i will do all the pulls with this solvent. I will post some pics of this when i do this. I have just finished re-exing the yeild from the two heptane pulls in 25ml of fresh heptane and ended up with 407mg of pure white crystal shards and a blob of yellow goo. and when the world stops
you will find me there
waiting to embrace you
|
|
|
Rennasauce Man
Posts: 853 Joined: 27-May-2011 Last visit: 25-Feb-2019 Location: A Pale Blue Dot orbiting a GV2 Yellow Dwarf fusion powered Luminous Ball of Plasma at 30km/s
|
Kerberos wrote:mrdruid0 wrote:So, you can totally substitute Naphtha in Cyb's for that pure Heptane?
I was thinking I may have to do this but I am really too unclear on how to go about it, would you mind clarifying on how you managed it? I warmed the Heptane, 50ml, and added it instead of the naphtha. I did this twice just as an experiment. The Heptane was then put in a pyrex dish and allowed to evaporate overnight. I scraped together the resulting crystals which were in the main very clean with a slightly yellow residue on the base of the dish. From two pulls i got 612mg using Cybs tek with 50g of MHRB. (I did another 4 pulls with naphtha and these are in the freezer.) So just substitute the word Heptane for the word Naphtha in the tek and your good to go. I dont know if you can freeze precip Heptane hopefully someone will chime in with this info. I will be doing Cybs tek again but this time i am going to use isoHexane and i will do all the pulls with this solvent. I will post some pics of this when i do this. I have just finished re-exing the yeild from the two heptane pulls in 25ml of fresh heptane and ended up with 407mg of pure white crystal shards and a blob of yellow goo. You answered your own question about re-x/freeze precip in heptane, but i'd like to chime in and say it works very well. I've replaced naptha, with a limo/fasw acid base, then rebase and re-x with minimal hot heptane. I've gotten ~1g of white crystals out of about 2.2 grams of heavily purified full spectrum fumarates from an limo/fasw acid base extraction on mhrb. You only need ~15-20ml of heptane when its near boiling hot (be careful obviously), to dissolve alot (i'd say about a gram) of dmt. It will cloud when you blow across the top, or when its cooled. Do it in a glass container, preferable a weighing jar with a g/g top, or a shot glass with something to seal the top with. Lots of crystals, and easy to recover. Then just evap until cloudy at room temp, and repeat until you have almost no heptane left. Evap that for yellowish waxy crystals that are just as good as the white stuff. I love heptane, naptha & I never really got along much, and i didn't really get into freeze precips/re-x's until i picked up a quart of heptane. "let those who have talked to the elves, find each other and band together" -TMK
In a society in which nearly everybody is dominated by somebody else's mind or by a disembodied mind, it becomes increasingly difficult to learn the truth about the activities of governments and corporations, about the quality or value of products, or about the health of one's own place and economy.
In such a society, also, our private economies will depend less upon the private ownership of real, usable property, and more upon property that is institutional and abstract, beyond individual control, such as money, insurance policies, certificates of deposit, stocks, etc. And as our private economies become more abstract, the mutual, free helps and pleasures of family and community life will be supplanted by a kind of displaced citizenship and by commerce with impersonal and self-interested suppliers...
The great enemy of freedom is the alignment of political power with wealth. This alignment destroys the commonwealth - that is, the natural wealth of localities and the local economies of household, neighborhood, and community - and so destroys democracy, of which the commonwealth is the foundation and practical means.โ - Wendell Berry
|
|
|
Michael
Posts: 175 Joined: 01-Nov-2010 Last visit: 10-Dec-2024 Location: UK
|
The Day Tripper wrote:You answered your own question about re-x/freeze precip in heptane, but i'd like to chime in and say it works very well. Hi The day tripper, i have never freeze precipitated Heptane, i have always evaped then re-ex. I do this by putting all the goods in hot Heptane then decanting the clean heptane into another shot glass leaving behind the yellow goo for later use. The clean heptane is then cling filmed and placed in a hot food flask to cool slowly. This results in very clean crystals which i recover by pouring off the heptane which i use again. I will post a couple of pics of my most successful crystal growing when i get home. and when the world stops
you will find me there
waiting to embrace you
|
|
|
Mr Invisible
Posts: 43 Joined: 12-May-2013 Last visit: 30-May-2013 Location: Orions Belt
|
Ah me bollocks... ok just recieved tetrosyl panel wipe and did a msds search for the part number and now i have found that it looks to be naphtha not hexane here is an updated msds "It Never Got Weird Enough For Me"..... But I Have A Feeling I'm About To Reach A Whole New Fucking Level!!!!
|
|
|
DMT-Nexus member
Posts: 4031 Joined: 28-Jun-2012 Last visit: 05-Mar-2024
|
MrInvisible wrote:Ah me bollocks... ok just recieved tetrosyl panel wipe and did a msds search for the part number and now i have found that it looks to be naphtha not hexane here is an updated msds This is the tetrosyl panel wipe msds, date 2007.: MSDS Tetrosyl Panel WipeProduct numbers: NPW005, PWS025, PWS050, PWS201, THIN09, THIN10, MFS050, PWD005, PWD250It says N-hexane, EC 203-777-6 So this one ^^^ is out dated, thanks for mentioning. Your file is 2011, Product numbers: NPW005, PWD005, PWD250Naphta, EC 265-151-9 <--- different product I've tried to find more about EC 265-151-9 here: a max boiling point of 60deg C, well that sounds not bad because hexane has a boiling point of 69 deg C, heptane 99 deg C. It looks even more volatile than hexane.
|
|
|
DMT-Nexus member
Posts: 1892 Joined: 05-Oct-2010 Last visit: 02-Oct-2024
|
It ain't called panel wipe suckas, where did i even mention this ? Art Van D'lay wrote:Smoalk. It. And. See.
|
|
|
Mr Invisible
Posts: 43 Joined: 12-May-2013 Last visit: 30-May-2013 Location: Orions Belt
|
hello i think it was me that mentioned the panel wipe... still in the moving house process... so not had a chance to do it yet.... i does evaporate cleanly though  "It Never Got Weird Enough For Me"..... But I Have A Feeling I'm About To Reach A Whole New Fucking Level!!!!
|
|
|
DMT-Nexus member
Posts: 4031 Joined: 28-Jun-2012 Last visit: 05-Mar-2024
|
When it comes to liquid hydrocarbons most refuse to ship overseas, maybe this works because of the aluminium bottles?
|
|
|
DMT-Nexus member
Posts: 220 Joined: 11-Apr-2013 Last visit: 06-Oct-2013 Location: The Nexus
|
I have to agree with DeMenTed on this one.
|