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How many times should you HCL salt from xylene? Options
 
Binary Drool
#1 Posted : 4/25/2013 3:12:22 AM

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Is once enough?
We actually worship incomprehensibility as the highest form of explanation. ~TM
 

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Kash
#2 Posted : 4/25/2013 3:39:08 AM

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Yes once is enough so long as enough salting volume is used and enough acid to properly titrate the xylene/aqueous solution. Second time you will only get a trace amount of alks, so it is really optional, SWIM usually skips it.
--------------------------------------------------*Kash's LSA Extraction* * Kash's Mescaline Extraction*------------------------------------------------------
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dg
#3 Posted : 4/25/2013 9:36:22 PM
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yeah-once is plenty if you just bring the water/hcl layer to ph 6
ph test the water layer not the np -in between small additions of acidic water and shaking
 
 
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