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bassterd
#1 Posted : 4/9/2013 10:51:07 AM
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Posts: 4
Joined: 21-Mar-2013
Last visit: 03-Nov-2013
Very excited to be a part of this site Razz i just started getting into dmt and extracting it, but ive had experience with other psychedelics.

Having a few problems with the extraction though, which is the main reason why i joined this site, so hopefully i can get some help form all the super knowledgable people here! Very happy

 

Good quality Syrian rue (Peganum harmala) for an incredible price!
 
Earthlova
#2 Posted : 4/9/2013 11:26:06 AM

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Posts: 105
Joined: 10-Mar-2011
Last visit: 06-Jul-2015
Location: North earth
Welcome bassterd Big grin
I am sure you will get the help you neededVery happy
 
bassterd
#3 Posted : 4/10/2013 12:32:21 PM
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Posts: 4
Joined: 21-Mar-2013
Last visit: 03-Nov-2013
So since I'm totally new to this forum, and forums in general, please excuse me if i posted this in the wrong place...

But i wanna post some pics of my project, maybe some of you can shed some light on it? I'll give a brief explanation of what happened.

Did a STB extraction, but got some nasty emulsions that just WOULDN'T go away, plus colorants in the solvent so when i preciped it i got brown sandy product. So i dissolved all of my pulls in some heptane and sucked the solvent off the dirty stuff that sank to the bottom.

I then proceeded to acid wash it with 24% vinegar (yes strong i know...) but was left with some slimy, membrany looking stuff that settled in the heptane layer. it was completely white, so i thought it was just undissolved spice that couldn't get into the already saturated solvent. However when i froze it, it still looked like that. I¨m pretty sure its still got lye in it.

So then i just poured all of the solvent back into a jar and tried to wash it with some water to get any of the lye out, but that didn't really help. Now i have a mason jar of basic water with white stuff that is floating on the top (which i thought was lye). and in my solvent jar i have a bunch of white stuff at the bottom of the jar. I really have no idea what to do now...The top layer in the mason jar is non-polar i think, since i can see the layer a bit through all of the white stuff.
bassterd attached the following image(s):
2013-04-10 11.07.20.jpg (1,506kb) downloaded 8 time(s).
2013-04-10 11.07.12.jpg (1,524kb) downloaded 7 time(s).
 
 
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