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acetone as a solvent idea Options
 
infinitelove
#1 Posted : 4/7/2013 4:11:06 AM

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I had some MHRB sitting in some sodium hydroxide water & decided to scrape off some of the residue(small crystals were formed) on the sides of the container into a cup...I then mixed some acetone into the powder and heated it up via double boiling...I'm letting the cup sit for a little while in the water but I'm going to eventually filter it with a coffee filter and let evaporate...
has anyone tried this and ended up with a good yield or even tried this at all???
I'd love some feedback Smile

I haven't stumbled across an already existing thread related to this already, I've searched... but if anyone has a link to one it would be greatly appreciated if you could post it here. Thank you. <3

I'm hoping this was a productive idea...
 

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infinitelove
#2 Posted : 4/8/2013 1:13:14 AM

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This will be a contribution post i guess, haha Smile
The results were good and crystals formed although not very pure/large...
thinking about using heptane for recrystallization, i'm hoping it'll work out well...it should.
I'll post results
 
remediosvaro
#3 Posted : 4/8/2013 1:03:50 PM

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it could be sodium hydroxide? definitely recrystallize in a np solvent
 
 
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